Technology Process of 2-Propenoyl chloride, 3-[4-(methylsulfonyl)phenyl]-, (E)-
There total 5 articles about 2-Propenoyl chloride, 3-[4-(methylsulfonyl)phenyl]-, (E)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: sodium hydride / tetrahydrofuran / 0.17 h / 0 °C
1.2: 2 h / 0 - 20 °C
2.1: sodium hydroxide; water monomer / ethanol / 1 h / 50 °C
3.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C
With
oxalyl dichloride; water monomer; sodium hydride; N,N-dimethyl-formamide; sodium hydroxide;
In
tetrahydrofuran; ethanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: sodium hydroxide; water monomer / ethanol / 1 h / 50 °C
2: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C
With
oxalyl dichloride; water monomer; N,N-dimethyl-formamide; sodium hydroxide;
In
ethanol; dichloromethane;
- Guidance literature:
-
Multi-step reaction with 5 steps
1.1: 3-chloro-benzenecarboperoxoic acid; Sodium hydrogenocarbonate / dichloromethane / 19.33 h / 0 - 20 °C
2.1: hydrogenchloride / 1,4-dioxane / 0.33 h / 100 °C
3.1: sodium hydride / tetrahydrofuran / 0.17 h / 0 °C
3.2: 2 h / 0 - 20 °C
4.1: sodium hydroxide; water monomer / ethanol / 1 h / 50 °C
5.1: oxalyl dichloride; N,N-dimethyl-formamide / dichloromethane / 1 h / 20 °C
With
hydrogenchloride; oxalyl dichloride; water monomer; sodium hydride; Sodium hydrogenocarbonate; N,N-dimethyl-formamide; 3-chloro-benzenecarboperoxoic acid; sodium hydroxide;
In
tetrahydrofuran; 1,4-dioxane; ethanol; dichloromethane;
