C₁₃H₁₃BrN₂OS

Base Information

Chemical Name:C₁₃H₁₃BrN₂OS
CAS No.:1370656-90-8
Molecular Formula:C₁₃H₁₃BrN₂OS
Molecular Weight:325.229
Hs Code.:

C<sub>13</sub>H<sub>13</sub>BrN<sub>2</sub>OS

Synonyms:

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Chemical Property of C₁₃H₁₃BrN₂OS

Chemical Property:

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Technology Process of C₁₃H₁₃BrN₂OS

There total 6 articles about C₁₃H₁₃BrN₂OS which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1370656-89-5
C₁₂H₁₄BrNO₂

: 1370656-90-8
C₁₃H₁₃BrN₂OS

Guidance literature:: Multi-step reaction with 2 steps

1: sodium hydrogencarbonate / dichloromethane; water

2: N-ethyl-N,N-diisopropylamine / 70 °C

With sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; In dichloromethane; water;
DOI:10.1016/j.bmcl.2012.02.013

Reference yield:

: 1049669-09-1
C₁₁H₁₂BrNO₂

: 1370656-90-8
C₁₃H₁₃BrN₂OS

Guidance literature:: Multi-step reaction with 3 steps

2: sodium hydrogencarbonate / dichloromethane; water

3: N-ethyl-N,N-diisopropylamine / 70 °C

With sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; In dichloromethane; water;
DOI:10.1016/j.bmcl.2012.02.013

Reference yield:

: 693774-26-4
(3-bromophenyl)(cyclopropyl)methanone

: 1370656-90-8
C₁₃H₁₃BrN₂OS

Guidance literature:: Multi-step reaction with 5 steps

1: potassium cyanide / 120 °C

2: water; potassium hydroxide / 24 h / 185 °C

4: sodium hydrogencarbonate / dichloromethane; water

5: N-ethyl-N,N-diisopropylamine / 70 °C

With potassium cyanide; water; sodium hydrogencarbonate; N-ethyl-N,N-diisopropylamine; potassium hydroxide; In dichloromethane; water; 1: Bucherer-Bergs reaction;
DOI:10.1016/j.bmcl.2012.02.013