(Ir(CO)(P(C₆H₅)3)(C₃H₃N₂))2*C₆H₁₄

Base Information

Chemical Name:(Ir(CO)(P(C₆H₅)3)(C₃H₃N₂))2*C₆H₁₄
CAS No.:92283-13-1
Molecular Formula:C₆H₁₄*C₄₄H₃₆Ir₂N₄O₂P₂
Molecular Weight:1185.36
Hs Code.:

(Ir(CO)(P(C<sub>6</sub>H<sub>5</sub>)3)(C<sub>3</sub>H<sub>3</sub>N<sub>2</sub>))2*C<sub>6</sub>H<sub>14</sub>

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Chemical Property of (Ir(CO)(P(C₆H₅)3)(C₃H₃N₂))2*C₆H₁₄

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Technology Process of (Ir(CO)(P(C₆H₅)3)(C₃H₃N₂))2*C₆H₁₄

There total 2 articles about (Ir(CO)(P(C₆H₅)3)(C₃H₃N₂))2*C₆H₁₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 101010-16-6
{Ir2(μ-η2-pyrazolate)2(η4-1,4-cyclooctadiene)2}

: 98420-38-3
dicarbonylbis(triphenylphosphine)bis(μ-pyrazolyl)diiridium(I)

: 92283-13-1
(Ir(CO)(P(C₆H₅)3)(C₃H₃N₂))2*C₆H₁₄

Guidance literature:: With CO; triphenylphosphine; In tetrahydrofuran; under N2, CO was bubbled through soln. of Ir-complex in THF, solvent removed, PPh3 in hexane was added, 15 min; concd., hexane added as upper layer;

Reference yield:

: 15318-31-7,14871-41-1,59246-46-7
bis(triphenylphosphine)iridium(I) carbonyl chloride

: 110-54-3
hexane

: 40958-82-5
sodium pyrazolide

: 98420-38-3
dicarbonylbis(triphenylphosphine)bis(μ-pyrazolyl)diiridium(I)

: 92283-13-1
(Ir(CO)(P(C₆H₅)3)(C₃H₃N₂))2*C₆H₁₄

Guidance literature:: In tetrahydrofuran; under N2, soln. of NaC3N2H3 in THF was added slowly to soln. of Ir-complex in THF, stirred at 25°C for 5 h; solvent removed, washed with hexane, dissolved in THF, filtered, concd., hexane added as upper layer, refrigerated; elem. anal.;