3-hexyl-phenylthiocyclopentanone

Base Information

Chemical Name:3-hexyl-phenylthiocyclopentanone
CAS No.:96994-78-4
Molecular Formula:C₁₇H₂₄OS
Molecular Weight:276.443
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-hexyl-phenylthiocyclopentanone

Chemical Property:

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Technology Process of 3-hexyl-phenylthiocyclopentanone

There total 2 articles about 3-hexyl-phenylthiocyclopentanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 34780-08-0
2-(phenylthio)cyclopent-2-en-1-one

: 3761-92-0
n-hexylmagnesium bromide

: 96994-78-4,96994-80-8
3-hexyl-phenylthiocyclopentanone

Guidance literature:: With copper(l) chloride; In tetrahydrofuran; for 0.666667h; Heating;

Reference yield:

: 34780-08-0
2-(phenylthio)cyclopent-2-en-1-one

: 21369-64-2
n-hexyllithium

: 86254-32-2
2-phenyl-sulphinyloct-1-en-3-one

: 96994-78-4,96994-80-8
3-hexyl-phenylthiocyclopentanone

Guidance literature:: With dimethylsulfide; copper(I) bromide; Yield given. Multistep reaction; 1.) hexane, THF, 0 deg C, 15 min; 2.) THF, 0 deg C, 45 min;

Reference yield:

: 96994-78-4,96994-80-8
3-hexyl-phenylthiocyclopentanone

: 96994-93-3,97059-01-3,97059-02-4,97059-03-5
15α-hydroxy-12β-phenylthio-1-nor-12α-prost-13-en-11-one

Guidance literature:: Multi-step reaction with 3 steps

2: trimethyl phosphite / toluene / 0.5 h

3: 36 percent / sodium cyanoborohydride, aq. HCl / tetrahydrofuran

With hydrogenchloride; sodium cyanoborohydride; phosphorous acid trimethyl ester; In tetrahydrofuran; toluene;