6-(p-methoxyphenyl)-3-oxo-2,4-diphenyl-3,3a,4,5-tetrahydrobenzopyrazole

Base Information

Chemical Name:6-(p-methoxyphenyl)-3-oxo-2,4-diphenyl-3,3a,4,5-tetrahydrobenzopyrazole
CAS No.:84725-20-2
Molecular Formula:C₂₆H₂₂N₂O₂
Molecular Weight:394.473
Hs Code.:

6-(p-methoxyphenyl)-3-oxo-2,4-diphenyl-3,3a,4,5-tetrahydrobenzo<c>pyrazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 6-(p-methoxyphenyl)-3-oxo-2,4-diphenyl-3,3a,4,5-tetrahydrobenzopyrazole

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Technology Process of 6-(p-methoxyphenyl)-3-oxo-2,4-diphenyl-3,3a,4,5-tetrahydrobenzopyrazole

There total 4 articles about 6-(p-methoxyphenyl)-3-oxo-2,4-diphenyl-3,3a,4,5-tetrahydrobenzopyrazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 84725-18-8,93938-47-7
4-carbomethoxy-1-(p-methoxyphenyl)-5-phenyl-cyclohex-1-en-3-one

: 100-63-0
phenylhydrazine

: 84725-20-2
6-(p-methoxyphenyl)-3-oxo-2,4-diphenyl-3,3a,4,5-tetrahydrobenzopyrazole

Guidance literature:: With acetic acid; In ethanol; for 3h; Heating;

Reference yield:

: 22966-19-4
trans-4'-methoxychalcone

: 84725-20-2
6-(p-methoxyphenyl)-3-oxo-2,4-diphenyl-3,3a,4,5-tetrahydrobenzopyrazole

Guidance literature:: Multi-step reaction with 2 steps

1: 77 percent / NaH, methanol / 3 h / Heating

2: 73 percent / acetic acid / ethanol / 3 h / Heating

With methanol; sodium hydride; acetic acid; In ethanol;

Reference yield:

: 100-52-7
benzaldehyde

: 84725-20-2
6-(p-methoxyphenyl)-3-oxo-2,4-diphenyl-3,3a,4,5-tetrahydrobenzopyrazole

Guidance literature:: Multi-step reaction with 3 steps

1: 70 percent / NaH, methanol / 1 h / Ambient temperature

2: 77 percent / NaH, methanol / 3 h / Heating

3: 73 percent / acetic acid / ethanol / 3 h / Heating

With methanol; sodium hydride; acetic acid; In ethanol;