5-Bromo-1-methoxy-2-nitro-3-propyl-benzene

Base Information

Chemical Name:5-Bromo-1-methoxy-2-nitro-3-propyl-benzene
CAS No.:94102-96-2
Molecular Formula:C₁₀H₁₂BrNO₃
Molecular Weight:274.114
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-Bromo-1-methoxy-2-nitro-3-propyl-benzene

Chemical Property:

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Technology Process of 5-Bromo-1-methoxy-2-nitro-3-propyl-benzene

There total 7 articles about 5-Bromo-1-methoxy-2-nitro-3-propyl-benzene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1700-37-4
3-Benzyloxybenzaldehyde

: 94102-96-2
5-Bromo-1-methoxy-2-nitro-3-propyl-benzene

Guidance literature:: Multi-step reaction with 6 steps

1: 1.) magnesium / 1.) diethyl ether, 2.) 0 deg C (1 h), room temperature (1 h), reflux (1 h)

2: 81 percent / hydrogen, hydrochloric acid / palladized charcoal / acetic acid

3: 75 percent / bromine, aluminium powder

4: 93 percent / aluminium chloride / benzene / 0.5 h / Heating

5: 24 percent / nitric acid / acetic acid / 10 - 15 °C

6: potassium carbonate / dimethylformamide / Ambient temperature

With hydrogenchloride; aluminium trichloride; hydrogen; bromine; nitric acid; potassium carbonate; magnesium; aluminium; palladium on activated charcoal; In acetic acid; N,N-dimethyl-formamide; benzene;

Reference yield:

: 55789-02-1
α-ethyl-3-hydroxybenzyl alcohol

: 94102-96-2
5-Bromo-1-methoxy-2-nitro-3-propyl-benzene

Guidance literature:: Multi-step reaction with 5 steps

1: 81 percent / hydrogen, hydrochloric acid / palladized charcoal / acetic acid

2: 75 percent / bromine, aluminium powder

3: 93 percent / aluminium chloride / benzene / 0.5 h / Heating

4: 24 percent / nitric acid / acetic acid / 10 - 15 °C

5: potassium carbonate / dimethylformamide / Ambient temperature

With hydrogenchloride; aluminium trichloride; hydrogen; bromine; nitric acid; potassium carbonate; aluminium; palladium on activated charcoal; In acetic acid; N,N-dimethyl-formamide; benzene;

Reference yield:

: 100-83-4
meta-hydroxybenzaldehyde

: 94102-96-2
5-Bromo-1-methoxy-2-nitro-3-propyl-benzene

Guidance literature:: Multi-step reaction with 7 steps

1: 78 percent / potassium carbonate / dimethylformamide / 7 h / Ambient temperature

2: 1.) magnesium / 1.) diethyl ether, 2.) 0 deg C (1 h), room temperature (1 h), reflux (1 h)

3: 81 percent / hydrogen, hydrochloric acid / palladized charcoal / acetic acid

4: 75 percent / bromine, aluminium powder

5: 93 percent / aluminium chloride / benzene / 0.5 h / Heating

6: 24 percent / nitric acid / acetic acid / 10 - 15 °C

7: potassium carbonate / dimethylformamide / Ambient temperature

With hydrogenchloride; aluminium trichloride; hydrogen; bromine; nitric acid; potassium carbonate; magnesium; aluminium; palladium on activated charcoal; In acetic acid; N,N-dimethyl-formamide; benzene;