2.3-DICHLOROBENZOTRICHLORIDE

Base Information

• Chemical Name: 2.3-DICHLOROBENZOTRICHLORIDE
• CAS No.: 84613-97-8
• Molecular Formula: C7H3 Cl5
• Molecular Weight: 264.366
• Hs Code.: 2903999090
• European Community (EC) Number: 283-395-4
• DSSTox Substance ID: DTXSID801004910
• Nikkaji Number: J140.753H
• Wikidata: Q83000139
• Mol file: 84613-97-8.mol

Synonyms:2.3-DICHLOROBENZOTRICHLORIDE;1,2-dichloro-3-(trichloromethyl)benzene

Chemical Property of 2.3-DICHLOROBENZOTRICHLORIDE

Chemical Property:

• PSA: 0.00000
• LogP: 4.82010
• XLogP3: 4.8
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 0
• Exact Mass: 263.864788
• Heavy Atom Count: 12
• Complexity: 152

Purity/Quality:

99% ^*data from raw suppliers

2,3-DICHLOROBENZOTRICHLORIDE 95.00% ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC(=C(C(=C1)Cl)Cl)C(Cl)(Cl)Cl

Technology Process of 2.3-DICHLOROBENZOTRICHLORIDE

There total 2 articles about 2.3-DICHLOROBENZOTRICHLORIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.6%

2,3-dichlorotoluene (32768-54-0) → 2,3-dichlorobenzotrichloride (84613-97-8)

Guidance literature:

With chlorine; In tetrachloromethane; at 75 ℃; Product distribution / selectivity; UV-irradiation;

Reference yield:

1,2-dichloro-benzene (95-50-1) → 2,3-dichlorobenzotrichloride (84613-97-8) + C13H6Cl6

Guidance literature:

With tetrachloromethane; C₆H₁₁N₂⁽¹⁺⁾*Cl^(1-)*AlCl₃; at 60 ℃; for 2h; under 760.051 Torr;

DOI:10.1007/s10562-018-2633-8

Reference yield: 88.0%

2,3-dichlorobenzotrichloride (84613-97-8) → 2,3-dichlorobenzoyl chloride (2905-60-4)

Guidance literature:

With water; zinc(II) chloride; at 160 - 165 ℃; for 1 - 7h; Product distribution / selectivity;

upstream raw materials:

2,3-dichlorotoluene

1,2-dichloro-benzene

Downstream raw materials:

2,3-dichlorobenzoyl chloride

2,3-dichloro-5-nitro-benzotrichloride

Refernces

• 1、 -. "METHOD FOR PREPARING LAMOTRIGINE AND ITS INTERMEDIATE 2,3-DICHLOROBENZOYL CHLORIDE". Page/Page column 13-14. . Retrieved 2010/11/29.