Technology Process of C27H34O2
There total 6 articles about C27H34O2 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 51 percent
2: Zn(Ag) / diethyl ether / Heating; var. reag.: Zn(Cu), d.e.> 80percent
With
silver; zinc;
In
diethyl ether;
DOI:10.1016/S0040-4039(00)95995-1
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 58 percent / pyridinium dichromate / CH2Cl2 / 10 h / Ambient temperature
2: 27 percent / a) HgCl2, Mg, b) TiCl4 / tetrahydrofuran / 24 h / 0 °C
3: 1.) BF3*Et2O or p-toluenesulfonic acid monohydrate, 2.) NaOMe / 1.) CH2Cl2, 0 deg C, 2.) DMSO, room temperature
4: Zn-Cu couple, K2CO3, iodine / diethyl ether / Heating
With
dipyridinium dichromate; boron trifluoride diethyl etherate; iodine; sodium methylate; titanium tetrachloride; copper; potassium carbonate; magnesium; mercury dichloride; zinc;
In
tetrahydrofuran; diethyl ether; dichloromethane;
DOI:10.1021/jo00294a016
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 27 percent / a) HgCl2, Mg, b) TiCl4 / tetrahydrofuran / 24 h / 0 °C
2: 1.) BF3*Et2O or p-toluenesulfonic acid monohydrate, 2.) NaOMe / 1.) CH2Cl2, 0 deg C, 2.) DMSO, room temperature
3: Zn-Cu couple, K2CO3, iodine / diethyl ether / Heating
With
boron trifluoride diethyl etherate; iodine; sodium methylate; titanium tetrachloride; copper; potassium carbonate; magnesium; mercury dichloride; zinc;
In
tetrahydrofuran; diethyl ether;
DOI:10.1021/jo00294a016