C₁₆H₁₄O₄

Base Information

• Chemical Name: C₁₆H₁₄O₄
• CAS No.: 387354-17-8
• Molecular Formula: C₁₆H₁₄O₄
• Molecular Weight: 270.285
• Mol file: 387354-17-8.mol

Synonyms:

Chemical Property of C₁₆H₁₄O₄

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₆H₁₄O₄

There total 1 articles about C₁₆H₁₄O₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-hydroxyphenylacetate (156-38-7) + 4-methoxy-benzaldehyde (123-11-5) → C16H14O4 (387354-17-8)

Guidance literature:

With acetic anhydride; triethylamine; at 130 - 140 ℃; for 6h;

DOI:10.1007/s00044-010-9369-3

Reference yield:

C16H14O4 (387354-17-8) → (E)-4-hydroxy-4'-methoxystilbene (65819-34-3,18951-44-5)

Guidance literature:

With copper; In quinoline; at 230 - 240 ℃; Inert atmosphere;

DOI:10.1002/chem.201303587

Reference yield:

C16H14O4 (387354-17-8) → C24H20O5

Guidance literature:

Multi-step reaction with 2 steps

1.1: sulfuric acid / 15 h / Inert atmosphere; Reflux

2.1: sodium hydride / N,N-dimethyl-formamide

2.2: 18 h / 80 °C

With sulfuric acid; sodium hydride; In N,N-dimethyl-formamide;

DOI:10.1007/s00044-010-9369-3

upstream raw materials:

4-hydroxyphenylacetate

4-methoxy-benzaldehyde

Downstream raw materials:

C₁₇H₁₆O₄

C₂₇H₂₃NO₆S

C₂₈H₂₅NO₆S

C₂₉H₂₇NO₆S