tetraphenyl-1,2-bis(trichloroacetoxy)distannane

Base Information

Chemical Name:tetraphenyl-1,2-bis(trichloroacetoxy)distannane
CAS No.:30872-44-7
Molecular Formula:C₂₈H₂₀Cl₆O₄Sn₂
Molecular Weight:870.602
Hs Code.:

Synonyms:

Suppliers and Price of tetraphenyl-1,2-bis(trichloroacetoxy)distannane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of tetraphenyl-1,2-bis(trichloroacetoxy)distannane

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of tetraphenyl-1,2-bis(trichloroacetoxy)distannane

There total 2 articles about tetraphenyl-1,2-bis(trichloroacetoxy)distannane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

: 1064-10-4
hexaphenylditin

: 76-03-9
trichloroacetic acid

: 30872-44-7
tetraphenyl-1,2-bis(trichloroacetoxy)distannane

Guidance literature:: In chloroform; byproducts: C6H6; Ph6Sn2 (5.0 mmol) dissolved in CHCl3, CCl3COOH (10.1 mmol) in CHCl3 added with stirring at room temp., stirred for 2 h at room temp.; cooled in refrigerator, fractional crystn. from CH2Cl2; elem. anal.;
DOI:10.1016/0022-328X(87)80155-9

Reference yield: 19.0%

: 1011-95-6
diphenyltin

: 76-03-9
trichloroacetic acid

: 30872-44-7
tetraphenyl-1,2-bis(trichloroacetoxy)distannane

Guidance literature:: In diethyl ether; byproducts: H2; to soln. of Ph2SnH2 (12.6 mmol) in ether added CCl3COOH (20.1 mmol), reacted for 16 h / A.K. Sawyer and H.G. Kuivila, J. Amer. Chem. Soc., 82 (1960) 5958; U.S.-Pat 3,083,217 (4.10.1960), ref. in C. A., 59 (1963) P7559c; J. Org. Chem., 27 (1962) 610;
DOI:10.1016/0022-328X(87)80155-9