Silane, trimethyl[3-methyl-1-[(4-methylphenyl)sulfonyl]-1,2-butadienyl]-

Base Information

Chemical Name:Silane, trimethyl[3-methyl-1-[(4-methylphenyl)sulfonyl]-1,2-butadienyl]-
CAS No.:136649-78-0
Molecular Formula:C15H22O2SSi
Molecular Weight:294.49
Hs Code.:
DSSTox Substance ID:DTXSID30455180
Mol file:136649-78-0.mol

Synonyms:136649-78-0;Silane, trimethyl[3-methyl-1-[(4-methylphenyl)sulfonyl]-1,2-butadienyl]-;DTXSID30455180

Suppliers and Price of Silane, trimethyl[3-methyl-1-[(4-methylphenyl)sulfonyl]-1,2-butadienyl]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Silane, trimethyl[3-methyl-1-[(4-methylphenyl)sulfonyl]-1,2-butadienyl]-

Chemical Property:

Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:3
Exact Mass:294.11097765
Heavy Atom Count:19
Complexity:473

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=C(C=C1)S(=O)(=O)C(=C=C(C)C)[Si](C)(C)C

Technology Process of Silane, trimethyl[3-methyl-1-[(4-methylphenyl)sulfonyl]-1,2-butadienyl]-

There total 2 articles about Silane, trimethyl[3-methyl-1-[(4-methylphenyl)sulfonyl]-1,2-butadienyl]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

: 75-77-4
chloro-trimethyl-silane

: 82352-39-4
1-<<3-methyl-1,2-Butadienyl>sulfonyl>-4-methylbenzene

: 136649-78-0
3-Methyl-1-(trimethylsilyl)buta-1,2-dien-1-yl p-tolyl sulfone

Guidance literature:: With n-butyllithium; In tetrahydrofuran; hexane; 1.) -78 deg C, 3 h, 2.) -78 deg C, 3 h;
DOI:10.1002/recl.19951140203

Reference yield:

: 10439-23-3
4-methylbenzenesulfinyl chloride

: 136649-78-0
3-Methyl-1-(trimethylsilyl)buta-1,2-dien-1-yl p-tolyl sulfone

Guidance literature:: Multi-step reaction with 3 steps

1: 91 percent / Et₃N / CH₂Cl₂ / 1.) -78 deg C, 2 h, 2.) 0 deg C, 1 h

2: 67 percent / 2,6-lutidine / acetonitrile / 6 h / Heating

3: 100 percent / n-BuLi / tetrahydrofuran; hexane / 1.) -78 deg C, 3 h, 2.) -78 deg C, 3 h

With 2,6-dimethylpyridine; n-butyllithium; triethylamine; In tetrahydrofuran; hexane; dichloromethane; acetonitrile;
DOI:10.1002/recl.19951140203