p-chlorobenzoyl-6 N,N-dimethyl gramine

Base Information

Chemical Name:p-chlorobenzoyl-6 N,N-dimethyl gramine
CAS No.:81223-94-1
Molecular Formula:C₁₈H₁₇ClN₂O
Molecular Weight:312.799
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of p-chlorobenzoyl-6 N,N-dimethyl gramine

Chemical Property:

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Technology Process of p-chlorobenzoyl-6 N,N-dimethyl gramine

There total 7 articles about p-chlorobenzoyl-6 N,N-dimethyl gramine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 50-00-0,30525-89-4,61233-19-0
formaldehyd

: 81223-74-7
p-chlorobenzoyl-6 indole

: 124-40-3
dimethyl amine

: 81223-94-1
p-chlorobenzoyl-6 N,N-dimethyl gramine

Guidance literature:: In methanol; for 120h; Heating;

Reference yield:

: 27428-57-5
4-bromo-4'-chlorobenzophenone

: 81223-94-1
p-chlorobenzoyl-6 N,N-dimethyl gramine

Guidance literature:: Multi-step reaction with 7 steps

1: 82 percent / p-TsOH / benzene / 48 h / Heating

2: 1) n-butyllithium / 1) ether, -30 deg C, 2 h, 2) -40 deg C

3: 51 percent / Na / methanol / 12 h / -10 °C

4: 74 percent / xylene / 3 h / Heating

5: 68 percent / aq. KOH / 2 h / Heating

6: 70 percent / copper chromite (barium promoted) / quinoline / 3 h / 220 °C

7: 40 percent / methanol / 120 h / Heating

With n-butyllithium; sodium; toluene-4-sulfonic acid; CuO/Cr₂O₃; In quinoline; methanol; potassium hydroxide; xylene; benzene;

Reference yield:

: 81223-63-4
dioxolanne de la chloro-4 bromo-4' benzophenone

: 81223-94-1
p-chlorobenzoyl-6 N,N-dimethyl gramine

Guidance literature:: Multi-step reaction with 6 steps

1: 1) n-butyllithium / 1) ether, -30 deg C, 2 h, 2) -40 deg C

2: 51 percent / Na / methanol / 12 h / -10 °C

3: 74 percent / xylene / 3 h / Heating

4: 68 percent / aq. KOH / 2 h / Heating

5: 70 percent / copper chromite (barium promoted) / quinoline / 3 h / 220 °C

6: 40 percent / methanol / 120 h / Heating

With n-butyllithium; sodium; CuO/Cr₂O₃; In quinoline; methanol; potassium hydroxide; xylene;