<1S,2S>-(+)-trans-2-methylcyclopentylphenyl ketone

Base Information

Chemical Name:<1S,2S>-(+)-trans-2-methylcyclopentylphenyl ketone
CAS No.:109583-31-5
Molecular Formula:C₁₃H₁₆O
Molecular Weight:188.269
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of <1S,2S>-(+)-trans-2-methylcyclopentylphenyl ketone

Chemical Property:

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Technology Process of <1S,2S>-(+)-trans-2-methylcyclopentylphenyl ketone

There total 3 articles about <1S,2S>-(+)-trans-2-methylcyclopentylphenyl ketone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 50.0%

: 75-09-2
dichloromethane

: 35660-91-4
(Z)-1-phenylbut-2-en-1-one

: 126525-21-1
(+/-)-(1'R,2'R)-(2'-methylcyclopropyl)phenyl methanone

: 18964-15-3,18964-16-4,100611-76-5,109583-31-5,140146-10-7,140146-11-8
(2‐methylcyclopentyl)(phenyl)methanone

Guidance literature:: With bis(acetylacetonate)nickel(II); C₁₆H₁₈N₂O; zinc; In N,N-dimethyl acetamide; at 22 ℃; Inert atmosphere; Glovebox;
DOI:10.1021/jacs.8b08296

Reference yield:

: 4885-02-3
Dichloromethyl methyl ether

: 109529-22-8
(trans-2-methylcyclopentyl)(phenyl)(isopropoxy)borane

: 18964-15-3,18964-16-4,100611-76-5,109583-31-5,140146-10-7,140146-11-8
(2‐methylcyclopentyl)(phenyl)methanone

Guidance literature:: With dihydrogen peroxide; lithium tert-butoxide; Yield given. Multistep reaction; 1.) diethyl ether, r.t., 1 h, 2.) diethyl ether, pH 8 phosphate buffer, 12 h;
DOI:10.1021/ja00252a018

Reference yield:

: 4885-02-3
Dichloromethyl methyl ether

: 109529-31-9
(<1S,2S>-trans-2-methylcyclopentyl)(phenyl)(3-(trimethylsiloxy)propoxy)borane

: 109583-31-5
<1S,2S>-(+)-trans-2-methylcyclopentylphenyl ketone

Guidance literature:: With dihydrogen peroxide; lithium tert-butoxide; Yield given. Multistep reaction; 1.) diethyl ether, r.t., 1 h, 2.) diethyl ether, pH 8 phosphate buffer, 12 h;
DOI:10.1021/ja00252a018