formic acid 3,4-bis-benzyloxy-5-chloro-phenyl ester

Base Information

Chemical Name:formic acid 3,4-bis-benzyloxy-5-chloro-phenyl ester
CAS No.:765950-74-1
Molecular Formula:C₂₁H₁₇ClO₄
Molecular Weight:368.817
Hs Code.:

Synonyms:

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Chemical Property of formic acid 3,4-bis-benzyloxy-5-chloro-phenyl ester

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Technology Process of formic acid 3,4-bis-benzyloxy-5-chloro-phenyl ester

There total 3 articles about formic acid 3,4-bis-benzyloxy-5-chloro-phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 34098-18-5
5-chloro-3,4-dihydroxybenzaldehyde

: 765950-74-1
formic acid 3,4-bis-benzyloxy-5-chloro-phenyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: 78 percent / KI; K₂CO₃ / acetone / 25 h / Heating

2: 3-chloroperoxybenzoic acid / CH₂Cl₂ / 18 h / Heating

With potassium carbonate; 3-chloro-benzenecarboperoxoic acid; potassium iodide; In dichloromethane; acetone;
DOI:10.1021/jo0491399

Reference yield:

: 19463-48-0
5-chlorovanillin

: 765950-74-1
formic acid 3,4-bis-benzyloxy-5-chloro-phenyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 94 percent / boron tribromide / CH₂Cl₂ / 4.3 h / 0 - 25 °C

2: 78 percent / KI; K₂CO₃ / acetone / 25 h / Heating

3: 3-chloroperoxybenzoic acid / CH₂Cl₂ / 18 h / Heating

With boron tribromide; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; potassium iodide; In dichloromethane; acetone;
DOI:10.1021/jo0491399

Reference yield:

: 121-33-5,8014-42-4
vanillin

: 765950-74-1
formic acid 3,4-bis-benzyloxy-5-chloro-phenyl ester

Guidance literature:: Multi-step reaction with 4 steps

1: 88 percent / chlorine / acetic acid / 0.5 h / 25 °C

2: 94 percent / boron tribromide / CH₂Cl₂ / 4.3 h / 0 - 25 °C

3: 78 percent / KI; K₂CO₃ / acetone / 25 h / Heating

4: 3-chloroperoxybenzoic acid / CH₂Cl₂ / 18 h / Heating

With chlorine; boron tribromide; potassium carbonate; 3-chloro-benzenecarboperoxoic acid; potassium iodide; In dichloromethane; acetic acid; acetone;
DOI:10.1021/jo0491399