(3S,4S,5R)-3,4,5-Trihydroxy-hexanoic acid N'-phenyl-hydrazide

Base Information

• Chemical Name: (3S,4S,5R)-3,4,5-Trihydroxy-hexanoic acid N'-phenyl-hydrazide
• CAS No.: 73491-12-0
• Molecular Formula: C₁₂H₁₈N₂O₄
• Molecular Weight: 254.286
• Mol file: 73491-12-0.mol

Synonyms:

Chemical Property of (3S,4S,5R)-3,4,5-Trihydroxy-hexanoic acid N'-phenyl-hydrazide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of (3S,4S,5R)-3,4,5-Trihydroxy-hexanoic acid N'-phenyl-hydrazide

There total 2 articles about (3S,4S,5R)-3,4,5-Trihydroxy-hexanoic acid N'-phenyl-hydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

boivinono-1,4-lactone (73522-67-5) + phenylhydrazine (100-63-0) → (3S,4S,5R)-3,4,5-Trihydroxy-hexanoic acid N'-phenyl-hydrazide (73491-12-0)

Guidance literature:

In ethanol; at 100 ℃; for 0.5h;

DOI:10.1016/S0008-6215(00)83840-9

Reference yield:

D-digitxose (527-52-6) → ribo-2,6-dideoxy-hexonic acid-(N'-phenyl-hydrazide) (20561-87-9,20561-91-5,20561-92-6,73491-12-0,83108-11-6,95103-71-2)

Guidance literature:

With water; bromine; levorotatory substance; Eindampfen der von Bromwasserstoff und Brom befreiten Loesung bei 50grad zum Sirup, diesen in Alkohol loesen und Hinzugeben von Phenylhydrazin;

upstream raw materials:

D-digitxose

boivinono-1,4-lactone

phenylhydrazine