(η5-cyclopentadienyl)dicarbonyl[(1-4-η)-5-phenylcyclohexadiene]molybdenum bromide

Base Information

• Chemical Name: (η5-cyclopentadienyl)dicarbonyl[(1-4-η)-5-phenylcyclohexadiene]molybdenum bromide
• CAS No.: 334698-95-2
• Molecular Formula: Br*C₁₉H₁₇MoO₂
• Molecular Weight: 453.187
• Mol file: 334698-95-2.mol

Synonyms:

Chemical Property of (η5-cyclopentadienyl)dicarbonyl[(1-4-η)-5-phenylcyclohexadiene]molybdenum bromide

Chemical Property:

Purity/Quality:

Safty Information:

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MSDS Files:

Useful:

Technology Process of (η5-cyclopentadienyl)dicarbonyl[(1-4-η)-5-phenylcyclohexadiene]molybdenum bromide

There total 1 articles about (η5-cyclopentadienyl)dicarbonyl[(1-4-η)-5-phenylcyclohexadiene]molybdenum bromide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

(η5-cyclopentadienyl)dicarbonyl[(2-4-η)-1-phenyl-2-cyclohexen-4-yl]molybdenum (334698-94-1) + di(p-anisyl)methyl bromide (69545-37-5) → (η5-cyclopentadienyl)dicarbonyl[(1-4-η)-5-phenylcyclohexadiene]molybdenum bromide (334698-95-2)

Guidance literature:

In dichloromethane; under Ar atm. to (η5-cyclopentadienyl)dicarbonyl((2-4-n)-1-phenyl-2-cyclohexen-4-yl)molybdenum in (CF3)2CHOH and CH2Cl2 at 0°C was added bromobis(4-methoxyphenyl)methane in CH2Cl2 and stirred at 0°Cfor 2 h; Et2O was added; elem. anal.;

DOI:10.1021/om000839n

upstream raw materials:

(η5-cyclopentadienyl)dicarbonyl[(2-4-η)-1-phenyl-2-cyclohexen-4-yl]molybdenum

di(p-anisyl)methyl bromide