(η5-cyclopentadienyl)dicarbonyl[(2-4-η)-1-phenyl-2-cyclohexen-4-yl]molybdenum

Base Information

Chemical Name:(η5-cyclopentadienyl)dicarbonyl[(2-4-η)-1-phenyl-2-cyclohexen-4-yl]molybdenum
CAS No.:334698-94-1
Molecular Formula:C₁₉H₁₈MoO₂
Molecular Weight:374.291
Hs Code.:

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Chemical Property of (η5-cyclopentadienyl)dicarbonyl[(2-4-η)-1-phenyl-2-cyclohexen-4-yl]molybdenum

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Technology Process of (η5-cyclopentadienyl)dicarbonyl[(2-4-η)-1-phenyl-2-cyclohexen-4-yl]molybdenum

There total 1 articles about (η5-cyclopentadienyl)dicarbonyl[(2-4-η)-1-phenyl-2-cyclohexen-4-yl]molybdenum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: (η(5)-cyclopentadienyl)dicarbonyl[(3,4,5,6-η)-cyclohexadiene]molybdenum hexafluorophosphate

: 100-58-3
phenylmagnesium bromide

: 334698-94-1
(η5-cyclopentadienyl)dicarbonyl[(2-4-η)-1-phenyl-2-cyclohexen-4-yl]molybdenum

Guidance literature:: In tetrahydrofuran; under Ar atm. to suspn. (η5-cyclopentadienyl)dicarbonyl((1-4-η)-cyclohexadiene)molybdenum hexafluorophosphate in THF at 0°C was added soln. PhMgBr in THF and stirred for 2 h at 0°C; saturated aq. NH4Cl was added, extd. with CH2Cl2, dried over Na2SO4, filtered, evapd., and chromed. (heptane/CH2Cl2 4:1);
DOI:10.1021/om000839n

Reference yield: 26.0%

: 334698-94-1
(η5-cyclopentadienyl)dicarbonyl[(2-4-η)-1-phenyl-2-cyclohexen-4-yl]molybdenum

: 69545-37-5
di(p-anisyl)methyl bromide

: 334698-95-2
(η5-cyclopentadienyl)dicarbonyl[(1-4-η)-5-phenylcyclohexadiene]molybdenum bromide

Guidance literature:: In dichloromethane; under Ar atm. to (η5-cyclopentadienyl)dicarbonyl((2-4-n)-1-phenyl-2-cyclohexen-4-yl)molybdenum in (CF3)2CHOH and CH2Cl2 at 0°C was added bromobis(4-methoxyphenyl)methane in CH2Cl2 and stirred at 0°Cfor 2 h; Et2O was added; elem. anal.;
DOI:10.1021/om000839n