Pd₂((C₆H₅)NCH(CH₃)CC(CH₃)NC₆H₅)2(CH₃COO)2

Base Information

Chemical Name:Pd₂((C₆H₅)NCH(CH₃)CC(CH₃)NC₆H₅)2(CH₃COO)2
CAS No.:1088447-11-3
Molecular Formula:C₃₈H₄₀N₄O₄Pd₂
Molecular Weight:829.6
Hs Code.:

Pd<sub>2</sub>((C<sub>6</sub>H<sub>5</sub>)NCH(CH<sub>3</sub>)CC(CH<sub>3</sub>)NC<sub>6</sub>H<sub>5</sub>)2(CH<sub>3</sub>COO)2

Synonyms:

Suppliers and Price of Pd₂((C₆H₅)NCH(CH₃)CC(CH₃)NC₆H₅)2(CH₃COO)2

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of Pd₂((C₆H₅)NCH(CH₃)CC(CH₃)NC₆H₅)2(CH₃COO)2

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of Pd₂((C₆H₅)NCH(CH₃)CC(CH₃)NC₆H₅)2(CH₃COO)2

There total 1 articles about Pd₂((C₆H₅)NCH(CH₃)CC(CH₃)NC₆H₅)2(CH₃COO)2 which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 88.3%

: PhNC(Me)CH₂C(Me)NPh

: 3375-31-3
palladium diacetate

: 1088447-11-3
Pd₂((C₆H₅)NCH(CH₃)CC(CH₃)NC₆H₅)2(CH₃COO)2

Guidance literature:: In acetone; byproducts: CH3COOH; soln. of diimine in acetone was added with stirring to soln. of Pd(OAc)2in acetone, stirred for 1.5 h; evapd. in vac., elem. anal.;
DOI:10.1021/ic801557c

Reference yield: 80.0%

: 1088447-11-3
Pd₂((C₆H₅)NCH(CH₃)CC(CH₃)NC₆H₅)2(CH₃COO)2

: potassium hydroxide

: (Pd((C₆H₅)NCH(CH₃)CC(CH₃)(C₆H₅)N)OH)2*2C₆H₆

Guidance literature:: In tetrahydrofuran; byproducts: KOOCCH3; KOH was added to soln. of palladium complex in THF, stirred for 2.5 h; filtered through celite, filtrate was evapd. in vac., extd. with benzene, filtered though celite, crystd.;
DOI:10.1021/ic801557c

Reference yield: 79.5%

: 1088447-11-3
Pd₂((C₆H₅)NCH(CH₃)CC(CH₃)NC₆H₅)2(CH₃COO)2

: 6046-93-1
copper(II) acetate monohydrate

: (Pd((C₆H₅)NCH(CH₃)CC(CH₃)(C₆H₅)N))2Cu(CH₃COO)4*2CH₂Cl₂

Guidance literature:: In tetrahydrofuran; to soln. of palladium complex in THF was added solid Cu(OAc)2*2H2O with stirring, stirred for 4 h at room temp.; filtered through celite, filtrate was evapd. in vac., dissolved in CH2Cl2, , layred with hexane, after several days crystals were collected, dried in air, elem. anal.;
DOI:10.1021/ic801557c