1,1-diphenyl-1-stannylcyclopent-3-ene

Base Information

Chemical Name:1,1-diphenyl-1-stannylcyclopent-3-ene
CAS No.:1147101-04-9
Molecular Formula:C₁₆H₁₆Sn
Molecular Weight:327.013
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,1-diphenyl-1-stannylcyclopent-3-ene

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Technology Process of 1,1-diphenyl-1-stannylcyclopent-3-ene

There total 1 articles about 1,1-diphenyl-1-stannylcyclopent-3-ene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 13.0%

: 753-73-1
dimethyltin dichloride

: 1135-99-5
diphenyltin(IV) dichloride

: 1147101-04-9
1,1-diphenyl-1-stannylcyclopent-3-ene

Guidance literature:: In tetrahydrofuran; (N2); suspn. of Mg compd. in THF was added dropwise over 4 h to stirred soln. of Sn compd. in THF at ambient temp.; when mixt. was neutral addition of Mg compd. was stopped; stirred for 15 min; evapd. (vac.); shaken with hexane; filtered; evapd. (vac.); chromd. (silica gel, hexane); elem. anal.;
DOI:10.1021/om800541f

Reference yield:

: 1147101-04-9
1,1-diphenyl-1-stannylcyclopent-3-ene

: 882-33-7
diphenyldisulfane

: 1103-05-5
bis(benzenethiolato-κ-S)diphenyltin(IV)

Guidance literature:: In benzene-d6; byproducts: butadiene; (N2); degassed mixt. of Sn compd. and Ph2S2 (16 equiv.) in C6D6 was sealed in NMR tube; heated at 100°C; NMR monitoring; not isolated; Kinetics;
DOI:10.1021/om800541f

Reference yield:

: 1147101-04-9
1,1-diphenyl-1-stannylcyclopent-3-ene

: dodecaphenylcyclohexastannane

Guidance literature:: In benzene-d6; byproducts: butadiene; (N2); soln. of Sn compd. in C6D6 was freeze-pump-thaw degassed; sealed; wrapped in Al foil; heated at 355.5 to 403.2 K; NMR monitoring; not isolated; Kinetics;
DOI:10.1021/om800541f