C₅₄H₇₁NO₄

Base Information

Chemical Name:C₅₄H₇₁NO₄
CAS No.:1402067-73-5
Molecular Formula:C₅₄H₇₁NO₄
Molecular Weight:798.162
Hs Code.:

C<sub>54</sub>H<sub>71</sub>NO<sub>4</sub>

Synonyms:

Suppliers and Price of C₅₄H₇₁NO₄

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₄H₇₁NO₄

Chemical Property:

Purity/Quality:

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MSDS Files:

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Technology Process of C₅₄H₇₁NO₄

There total 3 articles about C₅₄H₇₁NO₄ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 67-56-1
methanol

: 1402067-75-7
(4R)-4-((3R,5R,8R,9S,10S,12S,13R,17R)-3,12-bis(benzyloxy)-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)pentanal

: 103-49-1
dibenzylamine

: 1402067-80-4
(4R)-N,N-dibenzyl-4-((3R,5R,8R,9S,10S,12S,13R,17R)-3,12-bis(benzyloxy)-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)-1,1-dimethoxypentan-2-amine

: 1402067-73-5
C₅₄H₇₁NO₄

Guidance literature:: With sodium percarbonate; iodine; In dichloromethane; at 40 ℃; Overall yield = 85 %; Optical yield = 82 %de;
DOI:10.1002/anie.201204215

Reference yield:

: 83-44-3
Deoxycholic acid

: 1402067-80-4
(4R)-N,N-dibenzyl-4-((3R,5R,8R,9S,10S,12S,13R,17R)-3,12-bis(benzyloxy)-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)-1,1-dimethoxypentan-2-amine

: 1402067-73-5
C₅₄H₇₁NO₄

Guidance literature:: Multi-step reaction with 4 steps

1: sulfuric acid / 20 °C

2: silver trifluoromethanesulfonate; 2,6-di-tert-butyl-pyridine / dichloromethane / 3 h / Reflux

3: lithium aluminium tetrahydride / tetrahydrofuran

4: iodine; sodium percarbonate / dichloromethane / 40 °C

With lithium aluminium tetrahydride; 2,6-di-tert-butyl-pyridine; sodium percarbonate; sulfuric acid; iodine; silver trifluoromethanesulfonate; In tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.201204215

Reference yield:

: 3245-38-3
methyl deoxycholate

: 1402067-80-4
(4R)-N,N-dibenzyl-4-((3R,5R,8R,9S,10S,12S,13R,17R)-3,12-bis(benzyloxy)-10,13-dimethylhexadecahydro-1H-cyclopenta[a]phenanthren-17-yl)-1,1-dimethoxypentan-2-amine

: 1402067-73-5
C₅₄H₇₁NO₄

Guidance literature:: Multi-step reaction with 3 steps

1: silver trifluoromethanesulfonate; 2,6-di-tert-butyl-pyridine / dichloromethane / 3 h / Reflux

2: lithium aluminium tetrahydride / tetrahydrofuran

3: iodine; sodium percarbonate / dichloromethane / 40 °C

With lithium aluminium tetrahydride; 2,6-di-tert-butyl-pyridine; sodium percarbonate; iodine; silver trifluoromethanesulfonate; In tetrahydrofuran; dichloromethane;
DOI:10.1002/anie.201204215