C₂₄H₄₇NO₄SSi₂

Base Information

Chemical Name:C₂₄H₄₇NO₄SSi₂
CAS No.:1421663-99-1
Molecular Formula:C₂₄H₄₇NO₄SSi₂
Molecular Weight:501.878
Hs Code.:

C<sub>24</sub>H<sub>47</sub>NO<sub>4</sub>SSi<sub>2</sub>

Synonyms:

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Chemical Property of C₂₄H₄₇NO₄SSi₂

Chemical Property:

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Technology Process of C₂₄H₄₇NO₄SSi₂

There total 8 articles about C₂₄H₄₇NO₄SSi₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₂H₁₉NO₄S

: 18162-48-6
tert-butyldimethylsilyl chloride

: 1421663-99-1
C₂₄H₄₇NO₄SSi₂

Guidance literature:: With 1H-imidazole; dmap; In acetonitrile; at 20 ℃; for 2h; Inert atmosphere;
DOI:10.1139/cjc-2012-0340

Reference yield:

: C₁₂H₁₅NO₄S

: 1421663-99-1
C₂₄H₄₇NO₄SSi₂

Guidance literature:: Multi-step reaction with 2 steps

1: lithium borohydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

2: 1H-imidazole; dmap / acetonitrile / 2 h / 20 °C / Inert atmosphere

With 1H-imidazole; dmap; lithium borohydride; In tetrahydrofuran; acetonitrile;
DOI:10.1139/cjc-2012-0340

Reference yield:

: 1421663-96-8
C₁₄H₁₇NO₃

: 1421663-99-1
C₂₄H₄₇NO₄SSi₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: cobalt(II) chloride hexahydrate / tetrahydrofuran; water; isopropyl alcohol / 20 °C

1.2: 0 - 20 °C / Inert atmosphere

2.1: lithium hexamethyldisilazane / hexane; tetrahydrofuran / 0.5 h / 0 °C / Inert atmosphere

2.2: 2 h / 0 - 20 °C / Inert atmosphere

3.1: boron tribromide / dichloromethane / 1 h / -78 - 20 °C / Inert atmosphere

3.2: 0 - 20 °C / Inert atmosphere

4.1: lithium borohydride / tetrahydrofuran / 0 - 20 °C / Inert atmosphere

5.1: 1H-imidazole; dmap / acetonitrile / 2 h / 20 °C / Inert atmosphere

With 1H-imidazole; dmap; lithium borohydride; cobalt(II) chloride hexahydrate; boron tribromide; lithium hexamethyldisilazane; In tetrahydrofuran; hexane; dichloromethane; water; isopropyl alcohol; acetonitrile;
DOI:10.1139/cjc-2012-0340