C₂₉H₂₅O₆P

Base Information

Chemical Name:C₂₉H₂₅O₆P
CAS No.:1601392-95-3
Molecular Formula:C₂₉H₂₅O₆P
Molecular Weight:500.488
Hs Code.:

C<sub>29</sub>H<sub>25</sub>O<sub>6</sub>P

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₂₉H₂₅O₆P

Chemical Property:

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Technology Process of C₂₉H₂₅O₆P

There total 7 articles about C₂₉H₂₅O₆P which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 53.0%

: 3240-34-4
[bis(acetoxy)iodo]benzene

: C₂₅H₂₁O₂P

: 1601392-93-1
C₂₇H₂₃O₄P

: 1601392-95-3
C₂₉H₂₅O₆P

Guidance literature:: With palladium diacetate; In trifluoroacetic acid; at 100 ℃;
DOI:10.1039/c4cc01238k

Reference yield:

: 4559-70-0
Diphenylphosphine oxide

: 1601392-93-1
C₂₇H₂₃O₄P

: 1601392-95-3
C₂₉H₂₅O₆P

Guidance literature:: Multi-step reaction with 3 steps

1: bis(dibenzylideneacetone)-palladium⁽⁰⁾; 1,3-bis-(diphenylphosphino)propane; N-ethyl-N,N-diisopropylamine / toluene / 96 h / 120 °C / Schlenk technique; Reflux

2: bis(dibenzylideneacetone)-palladium⁽⁰⁾; triphenylphosphine; potassium phosphate / 1,4-dioxane / 12 h / 105 °C / Schlenk technique; Inert atmosphere

3: palladium diacetate / trifluoroacetic acid / 100 °C

With potassium phosphate; 1,3-bis-(diphenylphosphino)propane; palladium diacetate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In 1,4-dioxane; toluene; trifluoroacetic acid;
DOI:10.1039/c4cc01238k

Reference yield:

: 583-55-1
1-Bromo-2-iodobenzene

: 1601392-93-1
C₂₇H₂₃O₄P

: 1601392-95-3
C₂₉H₂₅O₆P

Guidance literature:: Multi-step reaction with 3 steps

1: bis(dibenzylideneacetone)-palladium⁽⁰⁾; 1,3-bis-(diphenylphosphino)propane; N-ethyl-N,N-diisopropylamine / toluene / 96 h / 120 °C / Schlenk technique; Reflux

2: bis(dibenzylideneacetone)-palladium⁽⁰⁾; triphenylphosphine; potassium phosphate / 1,4-dioxane / 12 h / 105 °C / Schlenk technique; Inert atmosphere

3: palladium diacetate / trifluoroacetic acid / 100 °C

With potassium phosphate; 1,3-bis-(diphenylphosphino)propane; palladium diacetate; N-ethyl-N,N-diisopropylamine; triphenylphosphine; bis(dibenzylideneacetone)-palladium⁽⁰⁾; In 1,4-dioxane; toluene; trifluoroacetic acid;
DOI:10.1039/c4cc01238k