6,12-dibenzyl-5,6,7,8,10,11,12,13,19,20-decahydro-9,18,21-trithia-6,12-diaza-dibenzo[a,g]cycloheptadecene

Base Information

• Chemical Name: 6,12-dibenzyl-5,6,7,8,10,11,12,13,19,20-decahydro-9,18,21-trithia-6,12-diaza-dibenzo[a,g]cycloheptadecene
• CAS No.: 917607-40-0
• Molecular Formula: C₃₄H₃₈N₂S₃
• Molecular Weight: 570.887

Synonyms:

Chemical Property of 6,12-dibenzyl-5,6,7,8,10,11,12,13,19,20-decahydro-9,18,21-trithia-6,12-diaza-dibenzo[a,g]cycloheptadecene

Chemical Property:

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Technology Process of 6,12-dibenzyl-5,6,7,8,10,11,12,13,19,20-decahydro-9,18,21-trithia-6,12-diaza-dibenzo[a,g]cycloheptadecene

There total 2 articles about 6,12-dibenzyl-5,6,7,8,10,11,12,13,19,20-decahydro-9,18,21-trithia-6,12-diaza-dibenzo[a,g]cycloheptadecene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.8%

benzyl bromide (100-39-0) + 5,6,7,8,10,11,12,13,19,20-decahydrodibenzo<1,4,11,8,14>-trithiadiazacycloheptadecine (113814-36-1) → 6,12-dibenzyl-5,6,7,8,10,11,12,13,19,20-decahydro-9,18,21-trithia-6,12-diaza-dibenzo[a,g]cycloheptadecene (917607-40-0)

Guidance literature:

With sodium hydrogencarbonate; In acetonitrile;

DOI:10.1039/b613636m

Reference yield:

2,2’-(ethane-1,2-diyldisulfanediyl)dibenzaldehyde (25676-67-9) → 6,12-dibenzyl-5,6,7,8,10,11,12,13,19,20-decahydro-9,18,21-trithia-6,12-diaza-dibenzo[a,g]cycloheptadecene (917607-40-0)

Guidance literature:

Multi-step reaction with 2 steps

1.1: ethanol / 3 h / Heating

1.2: 63 percent / sodium borohydride / ethanol / 12 h / Heating

2.1: 63.8 percent / sodium hydrogen carbonate / acetonitrile

With sodium hydrogencarbonate; In ethanol; acetonitrile;

DOI:10.1039/b613636m

Reference yield: 84.0%

6,12-dibenzyl-5,6,7,8,10,11,12,13,19,20-decahydro-9,18,21-trithia-6,12-diaza-dibenzo[a,g]cycloheptadecene (917607-40-0) + silver(I) hexafluorophosphate (26042-63-7) + acetonitrile (75-05-8,26809-02-9) → [Ag(S(C2H4N(CH2C6H5)CH2C6H4SCH2)2)](1+)*PF6(1-)*0.5CH3CN=[Ag(S(C2H4N(CH2C6H5)CH2C6H4SCH2)2)]PF6*0.5CH3CN

Guidance literature:

In acetonitrile; soln. of AgPF6 in MeCN was added to soln. of ligand in CH2Cl2; Et2O slowly diffused; filtered; washed (Et2O); crushed; dried (vac.); elem. anal.;

DOI:10.1039/b613636m

upstream raw materials:

benzyl bromide

5,6,7,8,10,11,12,13,19,20-decahydrodibenzo<1,4,11,8,14>-trithiadiazacycloheptadecine

2,2’-(ethane-1,2-diyldisulfanediyl)dibenzaldehyde

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