Ethyl 5-(2H-1,3-benzodioxol-5-yl)penta-2,4-dienoate

Base Information

Chemical Name:Ethyl 5-(2H-1,3-benzodioxol-5-yl)penta-2,4-dienoate
CAS No.:6091-43-6
Molecular Formula:C₁₄H₁₄O₄
Molecular Weight:246.263
Hs Code.:
DSSTox Substance ID:DTXSID10708323

Synonyms:63657-07-8;Ethyl 5-(2H-1,3-benzodioxol-5-yl)penta-2,4-dienoate;DTXSID10708323;KQDXOQJALDYLMO-UHFFFAOYSA-N;ethyl 5-(3,4-methylenedioxyphenyl)-2,4-pentadienoate

Suppliers and Price of Ethyl 5-(2H-1,3-benzodioxol-5-yl)penta-2,4-dienoate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Ethyl 5-(2H-1,3-benzodioxol-5-yl)penta-2,4-dienoate

Chemical Property:

XLogP3:3.4
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:246.08920892
Heavy Atom Count:18
Complexity:335

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOC(=O)C=CC=CC1=CC2=C(C=C1)OCO2

Technology Process of Ethyl 5-(2H-1,3-benzodioxol-5-yl)penta-2,4-dienoate

There total 13 articles about Ethyl 5-(2H-1,3-benzodioxol-5-yl)penta-2,4-dienoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: (E)-4-[(diethoxyphosphinyl)oxy]-2-butenoic acid ethyl ester

: 120-57-0,30024-74-9
piperonal

: 6091-43-6,56019-71-7,60578-08-7,60578-12-3,63657-07-8
all-trans-5-(3,4-Methylendioxyphenyl)-2,4-pentadiensaeureethylester

Guidance literature:: (E)-4-[(diethoxyphosphinyl)oxy]-2-butenoic acid ethyl ester; With sodium hydride; In N,N-dimethyl-formamide; at 30 - 35 ℃; for 4h;

piperonal; In N,N-dimethyl-formamide; at 20 ℃; for 16h;

Reference yield: 86.0%

: 120-57-0,30024-74-9
piperonal

: 42516-28-9
ethyl (2E)-4-(diethoxyphosphoryl)crotonate

: 6091-43-6,56019-71-7,60578-08-7,60578-12-3,63657-07-8
all-trans-5-(3,4-Methylendioxyphenyl)-2,4-pentadiensaeureethylester

Guidance literature:: With lithium hydroxide; In tetrahydrofuran; for 24h; Molecular sieve; Inert atmosphere; Reflux;
DOI:10.1016/j.bmc.2013.07.010