C₁₃H₁₅ClO

Base Information

Chemical Name:C₁₃H₁₅ClO
CAS No.:1431561-35-1
Molecular Formula:C₁₃H₁₅ClO
Molecular Weight:222.715
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₃H₁₅ClO

Chemical Property:

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Technology Process of C₁₃H₁₅ClO

There total 1 articles about C₁₃H₁₅ClO which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 58824-54-7
p-chlorophenylvinylcarbinol

: 78-84-2
isobutyraldehyde

: 1431561-35-1
C₁₃H₁₅ClO

Guidance literature:: With triethyl borane; palladium diacetate; triethylamine; triphenylphosphine; lithium chloride; In tetrahydrofuran; hexane; at 20 ℃; for 48h; Inert atmosphere;
DOI:10.1021/ja402893z

Reference yield:

: 1431561-35-1
C₁₃H₁₅ClO

: C₁₃H₁₈ClNO*C₂HF₃O₂

Guidance literature:: Multi-step reaction with 4 steps

1: hydroxylamine hydrochloride; sodium methylate / methanol / 14 h / Inert atmosphere; Reflux

2: sodium cyanoborohydride; acetic acid / dichloromethane / 1.08 h / 15 - 23 °C / Inert atmosphere; Sealed tube

3: triethylamine / dichloromethane / 14 h / 23 °C / Inert atmosphere; Sealed tube

4: dichloromethane / 1 h / 23 °C / Inert atmosphere

With hydroxylamine hydrochloride; sodium methylate; sodium cyanoborohydride; acetic acid; triethylamine; In methanol; dichloromethane;
DOI:10.1021/ja402893z

Reference yield:

: 1431561-35-1
C₁₃H₁₅ClO

: 1431561-41-9
(1E,4E)-5-(4-chlorophenyl)-2,2-dimethylpent-4-enal oxime

Guidance literature:: With hydroxylamine hydrochloride; sodium methylate; In methanol; for 14h; Inert atmosphere; Reflux;
DOI:10.1021/ja402893z