3'-<2-(Diphenylarsino)ethyl>spiro

Base Information

• Chemical Name: 3'-<2-(Diphenylarsino)ethyl>spiro
• CAS No.: 76124-29-3
• Molecular Formula: C₂₅H₂₃As
• Molecular Weight: 398.379
• Mol file: 76124-29-3.mol

Synonyms:

Chemical Property of 3'-<2-(Diphenylarsino)ethyl>spiro

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 3'-<2-(Diphenylarsino)ethyl>spiro

There total 3 articles about 3'-<2-(Diphenylarsino)ethyl>spiro which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-indene (95-13-6) → 3'-<2-(Diphenylarsino)ethyl>spiro (76124-29-3)

Guidance literature:

Multi-step reaction with 3 steps

1: 58 percent / NaNH₂ / tetrahydrofuran

2: 72 percent

3: 1) NaNH₂

With sodium amide; In tetrahydrofuran;

Reference yield:

<2-(3-Indenyl)ethyl>diphenylarsan (99475-13-5) + ethylene dibromide (106-93-4) → 3'-<2-(Diphenylarsino)ethyl>spiro (76124-29-3)

Guidance literature:

With sodium amide; Yield given. Multistep reaction;

Reference yield:

spiro(cyclopropane-1,1'-<1H>-indene) (19770-38-8) → 3'-<2-(Diphenylarsino)ethyl>spiro (76124-29-3)

Guidance literature:

Multi-step reaction with 2 steps

1: 72 percent

2: 1) NaNH₂

With sodium amide;

upstream raw materials:

<2-(3-Indenyl)ethyl>diphenylarsan

ethylene dibromide

spiro(cyclopropane-1,1'-<1H>-indene)

1-indene

Downstream raw materials:

1,3-Bis<2-(diphenylarsino)ethyl>inden