2'-(2-Methylbenzoyl)-2-naphthohydrazide

Base Information

Chemical Name:2'-(2-Methylbenzoyl)-2-naphthohydrazide
CAS No.:83803-94-5
Molecular Formula:C₁₉H₁₆N₂O₂
Molecular Weight:304.348
Hs Code.:2928000090
European Community (EC) Number:280-915-1
NSC Number:88892
DSSTox Substance ID:DTXSID80232680
Nikkaji Number:J296.273J
Wikidata:Q83113759

Synonyms:83803-94-5;2'-(2-Methylbenzoyl)-2-naphthohydrazide;2-(2-NAPHTHOYL)-1-(O-TOLUOYL)HYDRAZINE;N'-(2-methylbenzoyl)naphthalene-2-carbohydrazide;n'-(2-methylbenzoyl)-2-naphthohydrazide;EINECS 280-915-1;NSC88892;CBMicro_017697;DTXSID80232680;CCG-6313;MFCD00209665;NSC 88892;NSC-88892;AKOS003238740;BIM-0017658.P001;N'-(2-Methylbenzoyl)-2-naphthalenecarbohydrazide

Suppliers and Price of 2'-(2-Methylbenzoyl)-2-naphthohydrazide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
2-(2-NAPHTHOYL)-1-(O-TOLUOYL)HYDRAZINE 95.00%
5MG
$ 499.04

Total 10 raw suppliers

Chemical Property of 2'-(2-Methylbenzoyl)-2-naphthohydrazide

Chemical Property:

Vapor Pressure:8.71E-14mmHg at 25°C
Boiling Point:587.6°C at 760 mmHg
Flash Point:223.8°C
PSA：58.20000
Density:1.225g/cm³
LogP:4.00480
Sensitive.:Hygroscopic
XLogP3:4
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:2
Exact Mass:304.121177757
Heavy Atom Count:23
Complexity:437

Purity/Quality:

99% ^*data from raw suppliers

2-(2-NAPHTHOYL)-1-(O-TOLUOYL)HYDRAZINE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:
Statements: 36/37/38
Safety Statements: 26-37/39

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=CC=CC=C1C(=O)NNC(=O)C2=CC3=CC=CC=C3C=C2

Technology Process of 2'-(2-Methylbenzoyl)-2-naphthohydrazide

There total 3 articles about 2'-(2-Methylbenzoyl)-2-naphthohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.2%

: 39627-84-4
2-naphthohydrazide

: 933-88-0
ortho-toluoyl chloride

: 83803-94-5
2-methylbenzoic acid N'-(naphthalene-2-carbonyl)hydrazide

Guidance literature:: With sodium carbonate; In tetrahydrofuran; water; at 20 ℃; Cooling with ice;

Reference yield:

: 2459-25-8
methyl naphthalene-2-carboxylate

: 83803-94-5
2-methylbenzoic acid N'-(naphthalene-2-carbonyl)hydrazide

Guidance literature:: Multi-step reaction with 2 steps

1: hydrazine hydrate / ethanol / Reflux

2: sodium carbonate / tetrahydrofuran; water / 20 °C / Cooling with ice

With sodium carbonate; hydrazine hydrate; In tetrahydrofuran; ethanol; water;

Reference yield:

: 93-09-4
naphthalene-2-carboxylate

: 83803-94-5
2-methylbenzoic acid N'-(naphthalene-2-carbonyl)hydrazide

Guidance literature:: Multi-step reaction with 3 steps

1: sulfuric acid / Reflux

2: hydrazine hydrate / ethanol / Reflux

3: sodium carbonate / tetrahydrofuran; water / 20 °C / Cooling with ice

With sulfuric acid; sodium carbonate; hydrazine hydrate; In tetrahydrofuran; ethanol; water;