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Technology Process of H3NC(CH3)2CH2OH(1+)*VO2(1+)*H(1+)*C6H3(O)2CNHC(CH3)2CH2O(3-)=[H3NC(CH3)2CH2OH][VO2(C6H3(O)(OH)CNHC(CH3)2CH2O)]

H3NC(CH3)2CH2OH(1+)*VO2(1+)*H(1+)*C6H3(O)2CNHC(CH3)2CH2O(3-)=[H3NC(CH3)2CH2OH][VO2(C6H3(O)(OH)CNHC(CH3)2CH2O)]

Base Information
  • Chemical Name:H3NC(CH3)2CH2OH(1+)*VO2(1+)*H(1+)*C6H3(O)2CNHC(CH3)2CH2O(3-)=[H3NC(CH3)2CH2OH][VO2(C6H3(O)(OH)CNHC(CH3)2CH2O)]
  • CAS No.:167277-68-1
  • Molecular Formula:C4H12NO*C11H12NO3*H*O2V
  • Molecular Weight:380.315
  • Hs Code.:
H<sub>3</sub>NC(CH<sub>3</sub>)2CH<sub>2</sub>OH<sup>(1+)</sup>*VO<sub>2</sub><sup>(1+)</sup>*H<sup>(1+)</sup>*C<sub>6</sub>H<sub>3</sub>(O)2CNHC(CH<sub>3</sub>)2CH<sub>2</sub>O<sup>(3-)</sup>=[H<sub>3</sub>NC(CH<sub>3</sub>)2CH<sub>2</sub>OH][VO<sub>2</sub>(C<sub>6</sub>H<sub>3</sub>(O)(OH)CNHC(CH<sub>3</sub>)2CH<sub>2</sub>O)]

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Chemical Property of H3NC(CH3)2CH2OH(1+)*VO2(1+)*H(1+)*C6H3(O)2CNHC(CH3)2CH2O(3-)=[H3NC(CH3)2CH2OH][VO2(C6H3(O)(OH)CNHC(CH3)2CH2O)]
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Technology Process of H3NC(CH3)2CH2OH(1+)*VO2(1+)*H(1+)*C6H3(O)2CNHC(CH3)2CH2O(3-)=[H3NC(CH3)2CH2OH][VO2(C6H3(O)(OH)CNHC(CH3)2CH2O)]

There total 1 articles about H3NC(CH3)2CH2OH(1+)*VO2(1+)*H(1+)*C6H3(O)2CNHC(CH3)2CH2O(3-)=[H3NC(CH3)2CH2OH][VO2(C6H3(O)(OH)CNHC(CH3)2CH2O)] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 45.0%

2,5-Dihydroxybenzaldehyde
1194-98-5

2,5-Dihydroxybenzaldehyde

bis(acetylacetonate)oxovanadium
3153-26-2

bis(acetylacetonate)oxovanadium

2-Amino-2-methyl-1-propanol
124-68-5

2-Amino-2-methyl-1-propanol

2VO<sub>2</sub><sup>(1+)</sup>*2H<sub>2</sub>NC(CH<sub>3</sub>)2CH<sub>2</sub>O<sup>(1-)</sup>=[VO<sub>2</sub>(H<sub>2</sub>NC(CH<sub>3</sub>)2CH<sub>2</sub>O)]2

2VO2(1+)*2H2NC(CH3)2CH2O(1-)=[VO2(H2NC(CH3)2CH2O)]2

H<sub>3</sub>NC(CH<sub>3</sub>)2CH<sub>2</sub>OH<sup>(1+)</sup>*VO<sub>2</sub><sup>(1+)</sup>*H<sup>(1+)</sup>*C<sub>6</sub>H<sub>3</sub>(O)2CNHC(CH<sub>3</sub>)2CH<sub>2</sub>O<sup>(3-)</sup>=[H<sub>3</sub>NC(CH<sub>3</sub>)2CH<sub>2</sub>OH][VO<sub>2</sub>(C<sub>6</sub>H<sub>3</sub>(O)(OH)CNHC(CH<sub>3</sub>)2CH<sub>2</sub>O)]
167277-68-1

H3NC(CH3)2CH2OH(1+)*VO2(1+)*H(1+)*C6H3(O)2CNHC(CH3)2CH2O(3-)=[H3NC(CH3)2CH2OH][VO2(C6H3(O)(OH)CNHC(CH3)2CH2O)]

Guidance literature:
In methanol; stoich. amts.; refluxing aldehyde with aminoalcohol for 1 h, cooling toroom temp., addn. of V-compd., refluxing for 5 h; cooling, solvent removal (vac.), MeCN addn., pptn. on standing overnight (4°C), partial dissoln. in hot MeCN, repeated crystn. (MeCN); elem. anal.;
DOI:10.1039/DT9950002459

Reference yield:

H<sub>3</sub>NC(CH<sub>3</sub>)2CH<sub>2</sub>OH<sup>(1+)</sup>*VO<sub>2</sub><sup>(1+)</sup>*H<sup>(1+)</sup>*C<sub>6</sub>H<sub>3</sub>(O)2CNHC(CH<sub>3</sub>)2CH<sub>2</sub>O<sup>(3-)</sup>=[H<sub>3</sub>NC(CH<sub>3</sub>)2CH<sub>2</sub>OH][VO<sub>2</sub>(C<sub>6</sub>H<sub>3</sub>(O)(OH)CNHC(CH<sub>3</sub>)2CH<sub>2</sub>O)]
167277-68-1

H3NC(CH3)2CH2OH(1+)*VO2(1+)*H(1+)*C6H3(O)2CNHC(CH3)2CH2O(3-)=[H3NC(CH3)2CH2OH][VO2(C6H3(O)(OH)CNHC(CH3)2CH2O)]

VO<sup>(3+)</sup>*O<sub>2</sub><sup>(2-)</sup>*H<sup>(1+)</sup>*C<sub>6</sub>H<sub>3</sub>(O)2CNHC(CH<sub>3</sub>)2CH<sub>2</sub>O<sup>(3-)</sup>=VO(O<sub>2</sub>)(C<sub>6</sub>H<sub>3</sub>(O)(OH)CNHC(CH<sub>3</sub>)2CH<sub>2</sub>O)<sup>(1-)</sup>

VO(3+)*O2(2-)*H(1+)*C6H3(O)2CNHC(CH3)2CH2O(3-)=VO(O2)(C6H3(O)(OH)CNHC(CH3)2CH2O)(1-)

Guidance literature:
With H2O2; In N,N-dimethyl-formamide; varying excess of H2O2; not isolated, reaction followed by UV/VIS spectroscopy;
DOI:10.1039/DT9950002459
upstream raw materials:

2,5-Dihydroxybenzaldehyde

bis(acetylacetonate)oxovanadium

2-Amino-2-methyl-1-propanol

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