N,N-diethyl-N'-(+)-(3R)-menthyloxycarbonylthiourea

Base Information

Chemical Name:N,N-diethyl-N'-(+)-(3R)-menthyloxycarbonylthiourea
CAS No.:331823-15-5
Molecular Formula:C₁₆H₃₀N₂O₂S
Molecular Weight:314.492
Hs Code.:

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Chemical Property of N,N-diethyl-N'-(+)-(3R)-menthyloxycarbonylthiourea

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Technology Process of N,N-diethyl-N'-(+)-(3R)-menthyloxycarbonylthiourea

There total 1 articles about N,N-diethyl-N'-(+)-(3R)-menthyloxycarbonylthiourea which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 32.0%

: 7635-54-3,7635-53-2
(+)-(1S,2R,5S)-menthylchloroformate

: 333-20-0
potassium thioacyanate

: 109-89-7
diethylamine

: 331823-15-5
N,N-diethyl-N'-(+)-(3R)-menthyloxycarbonylthiourea

Guidance literature:: (+)-(1S,2R,5S)-menthylchloroformate; potassium thioacyanate; In acetone; for 2h; Heating;

diethylamine; In acetone; for 2h; Further stages.; Heating;
DOI:10.1039/b007589m

Reference yield: 64.0%

: 75992-73-3,25794-47-2,30729-25-0,15274-33-6,22840-91-1,14568-13-9
cis-dichlorobis(dimethylsulfoxide)platinum(II)

: 331823-15-5
N,N-diethyl-N'-(+)-(3R)-menthyloxycarbonylthiourea

: [PtCl((C₂H₅)2NCSNCOOC₆H₉(CH₃)((CH₃)2CH))(CH₃SOCH₃)]

Guidance literature:: With NaCH₃COO; In water; dimethyl sulfoxide; acetonitrile; addn. dropwise of soln. of (C2H5)2NCSNHCOOC6H9(CH3)((CH3)2CH) (1 equiv.)in CH3CN to soln. of PtCl2(DMSO)2 (1 equiv.) in CH3CN-DMSO (1:1), addn. of NaCH3COO in water, stirring at room temp. for 3 days; addn. of water, cooling at 4°C overnight, extn. into ether, drying over MgSO4, evapn. to dryness under reduced pressure; elem. anal.;
DOI:10.1039/b007589m