2-methyl-N-(3,5-trifluoromethylbenzoyl)iminopyridinium ylide

Base Information

Chemical Name:2-methyl-N-(3,5-trifluoromethylbenzoyl)iminopyridinium ylide
CAS No.:1337984-77-6
Molecular Formula:C₁₅H₁₀F₆N₂O
Molecular Weight:348.248
Hs Code.:

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Chemical Property of 2-methyl-N-(3,5-trifluoromethylbenzoyl)iminopyridinium ylide

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Technology Process of 2-methyl-N-(3,5-trifluoromethylbenzoyl)iminopyridinium ylide

There total 2 articles about 2-methyl-N-(3,5-trifluoromethylbenzoyl)iminopyridinium ylide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 785-56-8
3,5-bis(trifluoromethyl)phenyl carboxylic acid chloride

: 51135-75-2
2-methylpyridine N-imine

: 1337984-77-6
2-methyl-N-(3,5-trifluoromethylbenzoyl)iminopyridinium ylide

Guidance literature:: 2-methylpyridine N-imine; With sodium hydroxide; In tetrahydrofuran; water; at 20 ℃; for 0.0833333h; Inert atmosphere;

3,5-bis(trifluoromethyl)phenyl carboxylic acid chloride; In tetrahydrofuran; water; for 5h; Inert atmosphere;
DOI:10.1021/jo201303x

Reference yield:

: 109-06-8
α-picoline

: 1337984-77-6
2-methyl-N-(3,5-trifluoromethylbenzoyl)iminopyridinium ylide

Guidance literature:: Multi-step reaction with 2 steps

1.1: O-(2,4-dinitrophenyl)hydroxylamine / tetrahydrofuran; water / 16 h / 40 °C / Inert atmosphere

2.1: sodium hydroxide / tetrahydrofuran; water / 0.08 h / 20 °C / Inert atmosphere

2.2: 5 h / Inert atmosphere

With O-(2,4-dinitrophenyl)hydroxylamine; sodium hydroxide; In tetrahydrofuran; water;
DOI:10.1021/jo201303x