C₁₄H₉O₄ClC₆H₁₄Si

Base Information

• Chemical Name: C₁₄H₉O₄ClC₆H₁₄Si
• CAS No.: 315241-30-6
• Molecular Formula: C₂₀H₂₃ClO₄Si
• Molecular Weight: 390.939
• Mol file: 315241-30-6.mol

Synonyms:

Chemical Property of C₁₄H₉O₄ClC₆H₁₄Si

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of C₁₄H₉O₄ClC₆H₁₄Si

There total 2 articles about C₁₄H₉O₄ClC₆H₁₄Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

o-chlorobenzoyl chloride (609-65-4) → C14H9O4ClC6H14Si (315241-30-6)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium hydroxyde / H₂O / 0.5 h / 20 °C

2: imidazole / CH₂Cl₂ / 0 - 20 °C

With 1H-imidazole; potassium hydroxide; In dichloromethane; water; 1: Substitution / 2: Silylation;

DOI:10.1021/ol006518p

Reference yield:

salicylic acid (69-72-7,25496-36-0,8052-31-1) → C14H9O4ClC6H14Si (315241-30-6)

Guidance literature:

Multi-step reaction with 2 steps

1: potassium hydroxyde / H₂O / 0.5 h / 20 °C

2: imidazole / CH₂Cl₂ / 0 - 20 °C

With 1H-imidazole; potassium hydroxide; In dichloromethane; water; 1: Substitution / 2: Silylation;

DOI:10.1021/ol006518p

Reference yield: 55.0%

(trimethylsilyl)methylenetriphenylphosphorane (3739-97-7,75089-45-1) + C14H9O4ClC6H14Si (315241-30-6) → 2'-Chloroflavone (116115-48-1)

Guidance literature:

In tetrahydrofuran; for 43h; Heating;

DOI:10.1021/ol006518p

upstream raw materials:

o-chlorobenzoyl chloride

salicylic acid

Downstream raw materials:

2'-Chloroflavone