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N-methyl-N-undecylaniline

Base Information
  • Chemical Name:N-methyl-N-undecylaniline
  • CAS No.:46997-98-2
  • Molecular Formula:C18H31N
  • Molecular Weight:261.451
  • Hs Code.:
N-methyl-N-undecylaniline

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Chemical Property of N-methyl-N-undecylaniline
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Technology Process of N-methyl-N-undecylaniline

There total 5 articles about N-methyl-N-undecylaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:
Guidance literature:
With 1,10-Phenanthroline; copper(I) bromide; In 1,4-dioxane; at 60 ℃; for 12h; Inert atmosphere; Schlenk technique;
DOI:10.1021/acs.orglett.0c04203

Reference yield: 26.0%

Guidance literature:
With 1,10-Phenanthroline; copper(I) bromide; In 1,4-dioxane; at 60 ℃; for 12h; Schlenk technique; Inert atmosphere;
Guidance literature:
Multi-step reaction with 2 steps
1.1: dmap; dihydrogen peroxide / dichloromethane / 0.17 h / -15 °C
1.2: -15 - -10 °C
2.1: copper(I) bromide; 1,10-Phenanthroline / 1,4-dioxane / 12 h / 60 °C / Inert atmosphere; Schlenk technique
With dmap; 1,10-Phenanthroline; dihydrogen peroxide; copper(I) bromide; In 1,4-dioxane; dichloromethane;
DOI:10.1021/acs.orglett.0c04203
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