2,2-diphenyl-1,3-dioxolane-4-metanol butanoate

Base Information

Chemical Name:2,2-diphenyl-1,3-dioxolane-4-metanol butanoate
CAS No.:139730-21-5
Molecular Formula:C₂₀H₂₂O₄
Molecular Weight:326.392
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 2,2-diphenyl-1,3-dioxolane-4-metanol butanoate

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Technology Process of 2,2-diphenyl-1,3-dioxolane-4-metanol butanoate

There total 2 articles about 2,2-diphenyl-1,3-dioxolane-4-metanol butanoate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 22195-38-6
4--2,2-diphenyl-1,3-dioxolane

: 156-54-7
sodium butyrate

: 139730-21-5
2,2-diphenyl-1,3-dioxolane-4-metanol butanoate

Guidance literature:: In N,N,N,N,N,N-hexamethylphosphoric triamide; at 140 ℃; for 1.5h;
DOI:10.1016/S0957-4166(00)82313-7

Reference yield:

: 119-61-9
benzophenone

: 139730-21-5
2,2-diphenyl-1,3-dioxolane-4-metanol butanoate

Guidance literature:: Multi-step reaction with 2 steps

1: 64 percent / toluene-4-sulphonic acid monohydrate / toluene / Heating

2: 78 percent / hexamethylphosphoric acid triamide / 1.5 h / 140 °C

With toluene-4-sulfonic acid; In N,N,N,N,N,N-hexamethylphosphoric triamide; toluene;
DOI:10.1016/S0957-4166(00)82313-7