N--N-methylanilin

Base Information

• Chemical Name: N--N-methylanilin
• CAS No.: 100449-21-6
• Molecular Formula: C₁₇H₁₉NSi
• Molecular Weight: 265.43
• Mol file: 100449-21-6.mol

Synonyms:

Chemical Property of N--N-methylanilin

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of N--N-methylanilin

There total 1 articles about N--N-methylanilin which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

Lithium (39857-79-9) + phenyldimethylsilyl chloride (768-33-2) → N--N-methylanilin (100449-21-6)

Guidance literature:

In diethyl ether; hexane; for 3h; Ambient temperature;

Reference yield: 72.0%

N--N-methylanilin (100449-21-6) + 4-methoxybenzonitrile oxide (15500-73-9) → 4-(Dimethylphenylsilyl)-3-(4-methoxyphenyl)-5-(methylphenylamino)isoxazol (125379-78-4)

Guidance literature:

In diethyl ether; for 15h; Ambient temperature;

Reference yield: 53.0%

methyl 2-oxo-2H-pyrane-3-carboxylate (25991-27-9) + N--N-methylanilin (100449-21-6) → 3--2-benzoesaeure-methylester (100449-23-8)

Guidance literature:

In toluene; for 8h; Heating;

upstream raw materials:

Lithium

phenyldimethylsilyl chloride

Downstream raw materials:

3--2-benzoesaeure-methylester

4-(Dimethylphenylsilyl)-3-(4-methoxyphenyl)-5-(methylphenylamino)isoxazol