m-Menth-3(8)-ene.

Base Information

• Chemical Name: m-Menth-3(8)-ene.
• CAS No.: 13828-34-7
• Molecular Formula: C10H18
• Molecular Weight: 138.253
• Hs Code.: 2902199090
• Mol file: 13828-34-7.mol

Synonyms:m-menth-3(8)-ene;m-Menth-3(8)-en;m-3(8)-Menthene;Cyclohexane,1-methyl-3-(1-methylethylidene);Isosylveterpinolen;Cyclohexane, 1-methyl-3-(1-methylethylidene)-;1-methyl-3-(1-methylethylidene)-cyclohexane;

Chemical Property of m-Menth-3(8)-ene.

Chemical Property:

• Refractive Index: 1.4670
• Boiling Point: 188.7°C (rough estimate)
• PSA: 0.00000
• Density: 0.8214
• LogP: 3.53290

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of m-Menth-3(8)-ene.

There total 7 articles about m-Menth-3(8)-ene. which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

D-limonene (5989-27-5,555-08-8,8022-90-0,9003-73-0,95327-98-3) → Terpinolene (586-62-9,69073-38-7) + carvacrol (499-75-2) + methyl-cyclopentane (96-37-7) + 1-methyl-3-(2-methylpropyl)cyclopentane (29053-04-1) + 1-methyl-3-(1-methylethylidene)cyclohexane (13828-34-7) + 1-Methyl-3-propylbenzene (1074-43-7) + carane (554-59-6) + C10H18

Guidance literature:

With palm oil; palladium-nickel on zeolite HZSM-5 (SiO₂/Al₂O₃ ratio: 197); at 280 ℃; for 2h; under 6000.6 Torr; Autoclave; Inert atmosphere;

DOI:10.1039/c5cc06601h

Reference yield:

cis-Carane (554-59-6,2778-68-9,6069-97-2,18968-23-5,18968-24-6,83572-76-3,103239-63-0) → p-4(8)-menthene (1124-27-2) + 1-methyl-3-(1-methylethylidene)cyclohexane (13828-34-7) + 3-p-menthene (500-00-5)

Guidance literature:

zeolite Tseokar-2; at 100 ℃; for 4h; Yield given;

Reference yield:

trans-Carane (554-59-6,2778-68-9,6069-97-2,18968-23-5,18968-24-6,83572-76-3,103239-63-0) → p-4(8)-menthene (1124-27-2) + trans-8-p-menthene (1124-25-0) + 1-methyl-3-(1-methylethylidene)cyclohexane (13828-34-7) + m-2-menthene (13828-32-5) + m-3-menthene (13828-33-6) + 3-p-menthene (500-00-5)

Guidance literature:

zeolite Tseokar-2; at 80 ℃; for 5h; Product distribution; various catalysts, temperature and time;

upstream raw materials:

cis-Carane

trans-Carane

D-limonene

Downstream raw materials:

3-Methylcyclohexanone

acetone

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