Technology Process of methyl 2-acrylate
There total 6 articles about methyl 2-acrylate which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
bis(benzonitrile)palladium(II) dichloride; triethylamine;
for 3h;
Ambient temperature;
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 84 percent / LiAlH4 / diethyl ether / 2 h / Ambient temperature
2: 2) sodium borohydride / 1) ethanol, RT, 16 h, 2) 1 h
3: 23 percent / Et3N / Pd(PhCN)2Cl2 / 3 h / Ambient temperature
With
sodium tetrahydroborate; lithium aluminium tetrahydride; triethylamine;
bis(benzonitrile)palladium(II) dichloride;
In
diethyl ether;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: triethylamine / CH2Cl2 / 1 h / -10 °C
2: dimethylsulfoxide / 2 h / 75 °C
3: 84 percent / LiAlH4 / diethyl ether / 2 h / Ambient temperature
4: 2) sodium borohydride / 1) ethanol, RT, 16 h, 2) 1 h
5: 23 percent / Et3N / Pd(PhCN)2Cl2 / 3 h / Ambient temperature
With
sodium tetrahydroborate; lithium aluminium tetrahydride; triethylamine;
bis(benzonitrile)palladium(II) dichloride;
In
diethyl ether; dichloromethane; dimethyl sulfoxide;