[1,8-bis(diphenylphosphino)naphthalene]dihydroboron triflate

Base Information

Chemical Name:[1,8-bis(diphenylphosphino)naphthalene]dihydroboron triflate
CAS No.:1186424-44-1
Molecular Formula:CF₃O₃S*C₃₄H₂₈BP₂
Molecular Weight:658.425
Hs Code.:

Synonyms:

Suppliers and Price of [1,8-bis(diphenylphosphino)naphthalene]dihydroboron triflate

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 0 raw suppliers

Chemical Property of [1,8-bis(diphenylphosphino)naphthalene]dihydroboron triflate

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Technology Process of [1,8-bis(diphenylphosphino)naphthalene]dihydroboron triflate

There total 3 articles about [1,8-bis(diphenylphosphino)naphthalene]dihydroboron triflate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

: 1186424-32-7
1,8-bis(diphenylphosphino)naphthalene-borane

: 333-27-7
methyl trifluoromethanesulfonate

: 1186424-44-1
[1,8-bis(diphenylphosphino)naphthalene]dihydroboron triflate

Guidance literature:: In tetrahydrofuran; byproducts: methane; under Ar; B complex treated with CF3SO3Me in THF at room temp. for 4 h;
DOI:10.1021/om900017n

Reference yield: 95.0%

: 13292-87-0
dimethylsulfide borane complex

: 153725-04-3
1,8?bis(diphenylphosphino)naphthalene

: 333-27-7
methyl trifluoromethanesulfonate

: 1186424-44-1
[1,8-bis(diphenylphosphino)naphthalene]dihydroboron triflate

Guidance literature:: In tetrahydrofuran; diethyl ether; under Ar; soln. of H3BSMe2 in Et2O added dropwise at room temp. to soln.of C10H6(PPh2)2 (molar ratio 1.2:1) in THF; stirred for 1 h; CF3SO3Me a dded; stirred for 4 h; solvent removed under reduced pressure; washed with Et2O;
DOI:10.1021/om900017n

Reference yield:

: 153725-04-3
1,8?bis(diphenylphosphino)naphthalene

: 1186424-44-1
[1,8-bis(diphenylphosphino)naphthalene]dihydroboron triflate

Guidance literature:: Multi-step reaction with 2 steps

1: tetrahydrofuran; diethyl ether

2: tetrahydrofuran

In tetrahydrofuran; diethyl ether;
DOI:10.1021/om900017n