[((p-chlorophenyl)Sb)2O(hydrogen t-butylphosphonate^(1-))2(t-butylphosphonic acid)4]

Base Information

• Chemical Name: [((p-chlorophenyl)Sb)2O(hydrogen t-butylphosphonate^(1-))2(t-butylphosphonic acid)4]
• CAS No.: 1207297-83-3
• Molecular Formula: C₃₆H₇₂Cl₂O₁₉P₆Sb₂
• Molecular Weight: 1309.2
• Mol file: 1207297-83-3.mol

Synonyms:

Chemical Property of [((p-chlorophenyl)Sb)2O(hydrogen t-butylphosphonate^(1-))2(t-butylphosphonic acid)4]

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of [((p-chlorophenyl)Sb)2O(hydrogen t-butylphosphonate^(1-))2(t-butylphosphonic acid)4]

There total 1 articles about [((p-chlorophenyl)Sb)2O(hydrogen t-butylphosphonate^(1-))2(t-butylphosphonic acid)4] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

(p-chlorophenyl)stibonic acid (62170-62-1) + tert-butylphosphonic acid (4923-84-6) → [((p-chlorophenyl)Sb)2O(hydrogen t-butylphosphonate(1-))2(t-butylphosphonic acid)4] (1207297-83-3)

Guidance literature:

In acetonitrile; Sb compd. and t-BuP(OH)2O added to MeCN; stirred for 24 h; filtered; crystd. from filtrate by slow evapn. for 1 wk; elem. anal.;

DOI:10.1039/b913467k

Reference yield: 5.0%

methanol (67-56-1) + [((p-chlorophenyl)Sb)2O(hydrogen t-butylphosphonate(1-))2(t-butylphosphonic acid)4] (1207297-83-3) + lithium methanolate (865-34-9) + copper diacetate (142-71-2) → [Cu3O5((p-chlorophenyl)Sb)2(t-butylphosphonate(2-))4(pyridine)3] + [Cu5Li4O6((p-chlorophenyl)Sb)4(t-butylphosphonate(2-))6(acetate)2(methoxide)4(methanol)4]

Guidance literature:

In methanol; High Pressure; under solvothermal conditions; Sb complex and Cu acetate added to MeOH and LiOMe; sealed in Parr digestion bomb; heated at 100°C for 12 h; cooled slowly; filtered; crystd. by slow evapn. of filtrate; elem. anal.;

DOI:10.1039/b913467k

upstream raw materials:

(p-chlorophenyl)stibonic acid

tert-butylphosphonic acid