N′-(4-fluorophenyl)benzamidine

Base Information

• Chemical Name: N′-(4-fluorophenyl)benzamidine
• CAS No.: 1236358-07-8
• Molecular Formula: C₁₃H₁₁FN₂
• Molecular Weight: 214.242

Synonyms:

Chemical Property of N′-(4-fluorophenyl)benzamidine

Chemical Property:

Purity/Quality:

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Technology Process of N′-(4-fluorophenyl)benzamidine

There total 2 articles about N′-(4-fluorophenyl)benzamidine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

benzonitrile (100-47-0) + 4-fluoroaniline (371-40-4) → N′-(4-fluorophenyl)benzamidine (1236358-07-8,21719-88-0)

Guidance literature:

With C₃₇H₅₆N₅O₂Si₂Yb⁽²⁺⁾; at 100 ℃; for 12h; Neat (no solvent); Inert atmosphere;

DOI:10.1039/c2dt30400g

Reference yield: 87.0%

benzamide (55-21-0,27208-38-4) + 4-fluoroaniline (371-40-4) → N′-(4-fluorophenyl)benzamidine (1236358-07-8,21719-88-0)

Guidance literature:

With trimethylaluminum; In toluene; at 110 ℃; for 3h; Inert atmosphere;

DOI:10.1002/ejoc.201402386

Reference yield: 83.0%

N′-(4-fluorophenyl)benzamidine (1236358-07-8,21719-88-0) + 1,3-diphenylbenzo[e]-[1,2,4]triazin-7(1H)-one (22751-79-7) → N′-(4-fluorophenyl)-N-(1,7-dihydro-7-oxo-1,3-diphenylbenzo[e][1,2,4]triazin-6-yl)benzimidamide (1459721-87-9)

Guidance literature:

With N-ethyl-N,N-diisopropylamine; In toluene; at 100 ℃; for 24h;

DOI:10.1039/c3ob41169a

upstream raw materials:

benzonitrile

4-fluoroaniline

benzamide

Downstream raw materials:

N′-(4-fluorophenyl)-N-(1,7-dihydro-7-oxo-1,3-diphenylbenzo[e][1,2,4]triazin-6-yl)benzimidamide

N-(7-oxo-1,3-diphenyl-1,7-dihydrobenzo[e][1,2,4]triazin-6-yl)benzamide

8-(4-fluorophenyl)-1,3,7-triphenyl-4,8-dihydro-1H-imidazo[4,5-g][1,2,4]benzotriazin-4-yl

N-(1,7-dihydro-7-oxo-1,3-diphenylbenzo[e][1,2,4]triazin-6-yl)-N′-phenylbenzimidamide

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