trans-dichloro[2,3-dihydro-3-(2-methoxyphenyl)-2-methyl-5-phenyl-1,2,4-oxadiazole-κN(4)][pyridine-κN(1)]platinum

Base Information

• Chemical Name: trans-dichloro[2,3-dihydro-3-(2-methoxyphenyl)-2-methyl-5-phenyl-1,2,4-oxadiazole-κN(4)][pyridine-κN(1)]platinum
• CAS No.: 1247794-15-5
• Molecular Formula: C₂₁H₂₁Cl₂N₃O₂Pt
• Molecular Weight: 613.403

Synonyms:

Chemical Property of trans-dichloro[2,3-dihydro-3-(2-methoxyphenyl)-2-methyl-5-phenyl-1,2,4-oxadiazole-κN(4)][pyridine-κN(1)]platinum

Chemical Property:

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Technology Process of trans-dichloro[2,3-dihydro-3-(2-methoxyphenyl)-2-methyl-5-phenyl-1,2,4-oxadiazole-κN(4)][pyridine-κN(1)]platinum

There total 4 articles about trans-dichloro[2,3-dihydro-3-(2-methoxyphenyl)-2-methyl-5-phenyl-1,2,4-oxadiazole-κN(4)][pyridine-κN(1)]platinum which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

pyridine (110-86-1) + trans-dichloro[2,3-dihydro-3-(2-methoxyphenyl)-2-methyl-5-phenyl-1,2,4-oxadiazole-κN(4)][7-nitro-1,3,5-triazaadamantane-κN(1)]platinum (1247793-93-6) → trans-dichloro[2,3-dihydro-3-(2-methoxyphenyl)-2-methyl-5-phenyl-1,2,4-oxadiazole-κN(4)][pyridine-κN(1)]platinum (1247794-15-5)

Guidance literature:

In chloroform; soln. Pt complex and pyridine in CHCl3 was stirred at 37°C for 96h; solvent was evapd., product was purified by column chromy. on silica (CH2Cl2-EtOAc 98:2); elem. anal.;

DOI:10.1039/c0dt00360c

Reference yield:

N-(2-methoxybenzylidene)methanamine N-oxide (33499-30-8) → trans-dichloro[2,3-dihydro-3-(2-methoxyphenyl)-2-methyl-5-phenyl-1,2,4-oxadiazole-κN(4)][pyridine-κN(1)]platinum (1247794-15-5)

Guidance literature:

Multi-step reaction with 3 steps

1: chloroform

2: chloroform

3: chloroform

In chloroform;

DOI:10.1039/c0dt00360c

Reference yield:

trans-(benzonitrile)-dichloro[2,3-dihydro-3-(2-methoxyphenyl)-2-methyl-5-phenyl-1,2,4-oxadiazole-κN(4)]platinum (1247793-74-3) → trans-dichloro[2,3-dihydro-3-(2-methoxyphenyl)-2-methyl-5-phenyl-1,2,4-oxadiazole-κN(4)][pyridine-κN(1)]platinum (1247794-15-5)

Guidance literature:

Multi-step reaction with 2 steps

1: chloroform

2: chloroform

In chloroform;

DOI:10.1039/c0dt00360c

upstream raw materials:

pyridine

trans-dichloro[2,3-dihydro-3-(2-methoxyphenyl)-2-methyl-5-phenyl-1,2,4-oxadiazole-κN(4)][7-nitro-1,3,5-triazaadamantane-κN(1)]platinum

N-(2-methoxybenzylidene)methanamine N-oxide

trans-(benzonitrile)-dichloro[2,3-dihydro-3-(2-methoxyphenyl)-2-methyl-5-phenyl-1,2,4-oxadiazole-κN(4)]platinum

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