(1,3-diphenylpropane)bis(tricarbonylchromium)

Base Information

Chemical Name:(1,3-diphenylpropane)bis(tricarbonylchromium)
CAS No.:108319-36-4
Molecular Formula:C₂₁H₁₆Cr₂O₆
Molecular Weight:468.346
Hs Code.:

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Chemical Property of (1,3-diphenylpropane)bis(tricarbonylchromium)

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Technology Process of (1,3-diphenylpropane)bis(tricarbonylchromium)

There total 1 articles about (1,3-diphenylpropane)bis(tricarbonylchromium) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 47.0%

: 1081-75-0
1,3-diphenylpropane

: 199620-14-9,13007-92-6
chromium⁽⁰⁾ hexacarbonyl

: 108319-36-4
(1,3-diphenylpropane)bis(tricarbonylchromium)

: 82066-92-0
(1,3-diphenylpropane)tricarbonylchromium

Guidance literature:: In tetrahydrofuran; dibutyl ether; refluxing equimolar amts. under Ar, 36h; cooling to room temp.; addn. of silica gel; evapn.; chromy. (dry packed silica column, hexane/ethyl acetate 90/10); evapn.; elution with neat ethyl acetate yields the bis(tricarbonylchromium) complex;
DOI:10.1021/ja00247a022

Reference yield:

: 108319-36-4
(1,3-diphenylpropane)bis(tricarbonylchromium)

: 1076-43-3
benzene-d6

: 38095-88-4
(benzene-d6)tricarbonylchromium

: 82066-92-0
(1,3-diphenylpropane)tricarbonylchromium

Guidance literature:: In benzene-d6; Cr-complex was heated in neat benzene-d6 at 170°C; rate consts. are given; (1)H NMR analysis of reaction mixt.; Kinetics;