Fp-FBF₃

Base Information

Chemical Name:Fp-FBF₃
CAS No.:76391-69-0
Molecular Formula:C₇H₅BF₄FeO₂
Molecular Weight:263.767
Hs Code.:

Synonyms:

Suppliers and Price of Fp-FBF₃

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Fp-FBF₃

Chemical Property:

Purity/Quality:

Safty Information:

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Technology Process of Fp-FBF₃

There total 1 articles about Fp-FBF₃ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: dicarbonyl(cyclopentadienyl)methyliron(II)

: 341-02-6
trityl tetrafluoroborate

: 76391-69-0
Fp-FBF₃

: Fe(η-C5H5)(CO)2(COMe)

: 87794-75-0
(η5-Cp)(CO)2FeC(CH3)OFe(CO)2(η5-Cp)(tetrafluoroborate)

: 43105-67-5
[tricarbonyl-π-cyclopentadienyliron] hexafluoroantimonate

: 5271-39-6
Triphenylethan

Guidance literature:: In dichloromethane; under Ar, Ph3CBF4 and Fe complex mixed in solid state, at 0°C added CH2Cl2, kept for 100 h from -10 to 10°C; ppt. centrifuged, washed with hexane, dried at room temp. in vac.;
DOI:10.1016/S0022-328X(00)99506-8

Reference yield: 19.0%

: 76391-69-0
Fp-FBF₃

: 922-67-8
propynoic acid methyl ester

: 501-65-5
diphenyl acetylene

: 714960-49-3
dicarbonylcyclopentadienyl-3-(2-methoxy-5,6-diphenylpyrylium)iron(II) tetrafluoroborate

Guidance literature:: In dichloromethane; (Ar); methyl propiolate was added via syringe to soln. of Fe complex in CH2Cl2; mixt. was stirred for 30 min; alkyne was added; soln. was stirred overnight; filtered through Celite; solvent removed (vac.); THF transferred (vac.) to residue; concd. (vac.); cooled to -30°C overnight; isolated byfilter cannulation; washed (Et2O); elem. anal.;
DOI:10.1021/om0343420

Reference yield: 19.0%

: 76391-69-0
Fp-FBF₃

: 536-74-3
phenylacetylene

: 922-67-8
propynoic acid methyl ester

: 714960-52-8
dicarbonylcyclopentadienyl-3-(2-methoxy-6-phenylpyrylium)iron(II) tetrafluoroborate

Guidance literature:: In dichloromethane; (Ar); methyl propiolate was added via syringe to soln. of Fe complex in CH2Cl2; mixt. was stirred for 30 min; alkyne was added; soln. was stirred overnight; filtered through Celite; solvent removed (vac.); THF transferred (vac.) to residue; concd. (vac.); cooled to -30°C overnight; isolated byfilter cannulation; washed (Et2O); elem. anal.;
DOI:10.1021/om0343420