bis(8-quinolyl)phenylsilane

Base Information

Chemical Name:bis(8-quinolyl)phenylsilane
CAS No.:1238358-95-6
Molecular Formula:C₂₄H₁₈N₂Si
Molecular Weight:362.506
Hs Code.:

Synonyms:

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Chemical Property of bis(8-quinolyl)phenylsilane

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Technology Process of bis(8-quinolyl)phenylsilane

There total 1 articles about bis(8-quinolyl)phenylsilane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 39.0%

: 16567-18-3
8-bromoquinoline

: 1631-84-1
dichlorophenylsilane

: 1238358-95-6
bis(8-quinolyl)phenylsilane

Guidance literature:: 8-bromoquinoline; With n-butyllithium; In tetrahydrofuran; hexane; at -78 ℃; for 0.166667h;

dichlorophenylsilane; In tetrahydrofuran; hexane; at -78 - 20 ℃;
DOI:10.1021/om1004622

Reference yield: 38.0%

: 1295-35-8
bis(1,5-cyclooctadiene)nickel ⁽⁰⁾

: 1238358-95-6
bis(8-quinolyl)phenylsilane

: 107-06-2,52399-93-6
1,2-dichloro-ethane

: (bis(8-quinolyl)phenylsilyl)2Ni₃Cl₂*0.5(1,2-dichloroethane)

Guidance literature:: In chlorobenzene; under N2; slurry of Si compd. in chlorobenzene added to Ni complex with stirring; stirred at room temp. for 1 d; concd.; pentane added; washed with pentane; dissolved in 1,2-dichloroethane; filtered through Celite and glass fiber filter; layered with pentane; crystd. at -30°C; elem. anal.;
DOI:10.1021/om1004622

Reference yield: 12.0%

: bis-allylnickel chloride

: 75-09-2
dichloromethane

: 1238358-95-6
bis(8-quinolyl)phenylsilane

: 1238359-06-2
(chlorobis(8-quinolyl)phenylsilane)NiCl*(dichloromethane)

: (bis(8-quinolyl)phenylsilyl)2Ni₃Cl₂

Guidance literature:: In dichloromethane; under N2; slurry of Si compd. in CH2Cl2 added dropwise to soln. of Ni complex in CH2Cl2; stirred at room temp. for 10 min; filtered; soln. layered with pentane at room temp. for 1 d; dissolved inCH2Cl2; filtered; layered with pentane; crystd. at room temp.; elem. an al.;
DOI:10.1021/om1004622