Technology Process of C19H26O6
There total 9 articles about C19H26O6 which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
sodium chlorite; sodium dihydrogenphosphate;
In
2-methyl-but-2-ene; water; tert-butyl alcohol;
at 0 ℃;
for 0.5h;
DOI:10.1039/c0ob01253j
- Guidance literature:
-
Multi-step reaction with 6 steps
1: acetic acid; zinc / ethanol / 2 h / 20 °C
2: 1H-imidazole / N,N-dimethyl-formamide / 6 h / 20 °C
3: camphor-10-sulfonic acid / dichloromethane / 20 °C
4: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C
5: sulfur trioxide pyridine complex; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 0 °C
6: sodium dihydrogenphosphate; sodium chlorite / 2-methyl-but-2-ene; water; tert-butyl alcohol / 0.5 h / 0 °C
With
1H-imidazole; sodium chlorite; sodium dihydrogenphosphate; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; sulfur trioxide pyridine complex; acetic acid; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine; zinc;
In
tetrahydrofuran; 2-methyl-but-2-ene; ethanol; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
5: Parikh-Doering oxidation;
DOI:10.1039/c0ob01253j
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 1H-imidazole / N,N-dimethyl-formamide / 6 h / 20 °C
2: camphor-10-sulfonic acid / dichloromethane / 20 °C
3: tetrabutyl ammonium fluoride / tetrahydrofuran / 20 °C
4: sulfur trioxide pyridine complex; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine / dichloromethane / 1 h / 0 °C
5: sodium dihydrogenphosphate; sodium chlorite / 2-methyl-but-2-ene; water; tert-butyl alcohol / 0.5 h / 0 °C
With
1H-imidazole; sodium chlorite; sodium dihydrogenphosphate; camphor-10-sulfonic acid; tetrabutyl ammonium fluoride; sulfur trioxide pyridine complex; dimethyl sulfoxide; N-ethyl-N,N-diisopropylamine;
In
tetrahydrofuran; 2-methyl-but-2-ene; dichloromethane; water; N,N-dimethyl-formamide; tert-butyl alcohol;
4: Parikh-Doering oxidation;
DOI:10.1039/c0ob01253j