(E)-1-(4-(azidomethoxy)phenyl)-2-(4-(4-iodophenylcarbamoyl)piperidin-1-yl)-2-oxoethyl 4-(4-((4-(dimethylamino)phenyl)diazenyl)benzamido)cyclohexylcarbamate

Base Information

Chemical Name:(E)-1-(4-(azidomethoxy)phenyl)-2-(4-(4-iodophenylcarbamoyl)piperidin-1-yl)-2-oxoethyl 4-(4-((4-(dimethylamino)phenyl)diazenyl)benzamido)cyclohexylcarbamate
CAS No.:1416550-04-3
Molecular Formula:C₄₃H₄₇IN₁₀O₆
Molecular Weight:926.814
Hs Code.:

(E)-1-(4-(azidomethoxy)phenyl)-2-(4-(4-iodophenylcarbamoyl)piperidin-1-yl)-2-oxoethyl 4-(4-((4-(dimethylamino)phenyl)diazenyl)benzamido)cyclohexylcarbamate

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Chemical Property of (E)-1-(4-(azidomethoxy)phenyl)-2-(4-(4-iodophenylcarbamoyl)piperidin-1-yl)-2-oxoethyl 4-(4-((4-(dimethylamino)phenyl)diazenyl)benzamido)cyclohexylcarbamate

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Technology Process of (E)-1-(4-(azidomethoxy)phenyl)-2-(4-(4-iodophenylcarbamoyl)piperidin-1-yl)-2-oxoethyl 4-(4-((4-(dimethylamino)phenyl)diazenyl)benzamido)cyclohexylcarbamate

There total 5 articles about (E)-1-(4-(azidomethoxy)phenyl)-2-(4-(4-iodophenylcarbamoyl)piperidin-1-yl)-2-oxoethyl 4-(4-((4-(dimethylamino)phenyl)diazenyl)benzamido)cyclohexylcarbamate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1160707-38-9
C₂₈H₂₅IN₆O₈

: (E)-N-(4-aminocyclohexyl)-4-((4-(dimethylamino)phenyl)diazenyl)benzamide trifluoroacetate

: 1416550-04-3
(E)-1-(4-(azidomethoxy)phenyl)-2-(4-(4-iodophenylcarbamoyl)piperidin-1-yl)-2-oxoethyl 4-(4-((4-(dimethylamino)phenyl)diazenyl)benzamido)cyclohexylcarbamate

Guidance literature:: With triethylamine; In dichloromethane; at 20 - 35 ℃;
DOI:10.1039/c2cc37826d

Reference yield:

: 201858-51-7
p-methyl red

: 1416550-04-3
(E)-1-(4-(azidomethoxy)phenyl)-2-(4-(4-iodophenylcarbamoyl)piperidin-1-yl)-2-oxoethyl 4-(4-((4-(dimethylamino)phenyl)diazenyl)benzamido)cyclohexylcarbamate

Guidance literature:: Multi-step reaction with 3 steps

1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / dichloromethane

2: hydrogenchloride / 2 h / 20 °C

3: triethylamine / dichloromethane / 20 - 35 °C

With hydrogenchloride; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; In dichloromethane;
DOI:10.1039/c2cc37826d

Reference yield:

: 1198-84-1
4-hydroxymandelic acid

: 1416550-04-3
(E)-1-(4-(azidomethoxy)phenyl)-2-(4-(4-iodophenylcarbamoyl)piperidin-1-yl)-2-oxoethyl 4-(4-((4-(dimethylamino)phenyl)diazenyl)benzamido)cyclohexylcarbamate

Guidance literature:: Multi-step reaction with 5 steps

1.1: 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; benzotriazol-1-ol / N,N-dimethyl-formamide

2.1: sodium iodide; potassium tert-butylate / N,N-dimethyl-formamide; tetrahydrofuran / 2 h / 20 °C

3.1: N-chloro-succinimide; chloro-trimethyl-silane / dichloromethane / 1.5 h

3.2: 1.5 h / 20 °C

4.1: triethylamine / dichloromethane / 4 h

5.1: triethylamine / dichloromethane / 20 - 35 °C

With N-chloro-succinimide; chloro-trimethyl-silane; potassium tert-butylate; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; sodium iodide; In tetrahydrofuran; dichloromethane; N,N-dimethyl-formamide;
DOI:10.1039/c2cc37826d