1-[2-hydroxy-2-(4-(methylthiomethoxy)phenyl)acetyl]-N-(4-iodophenyl)piperidine-4-carboxamide

Base Information

Chemical Name:1-[2-hydroxy-2-(4-(methylthiomethoxy)phenyl)acetyl]-N-(4-iodophenyl)piperidine-4-carboxamide
CAS No.:1160707-36-7
Molecular Formula:C₂₂H₂₅IN₂O₄S
Molecular Weight:540.422
Hs Code.:

Synonyms:1-[2-hydroxy-2-(4-(methylthiomethoxy)phenyl)acetyl]-N-(4-iodophenyl)piperidine-4-carboxamide

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Chemical Property of 1-[2-hydroxy-2-(4-(methylthiomethoxy)phenyl)acetyl]-N-(4-iodophenyl)piperidine-4-carboxamide

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Technology Process of 1-[2-hydroxy-2-(4-(methylthiomethoxy)phenyl)acetyl]-N-(4-iodophenyl)piperidine-4-carboxamide

There total 1 articles about 1-[2-hydroxy-2-(4-(methylthiomethoxy)phenyl)acetyl]-N-(4-iodophenyl)piperidine-4-carboxamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 78.0%

: 2373-51-5
chloro-methylsulfanyl-methane

: 1160707-35-6
1-[2-hydroxy-2-(4-hydroxyphenyl)acetyl]-N-(4-iodophenyl)piperidine-4-carboxamide

: 1160707-36-7
1-[2-hydroxy-2-(4-(methylthiomethoxy)phenyl)acetyl]-N-(4-iodophenyl)piperidine-4-carboxamide

Guidance literature:: 1-[2-hydroxy-2-(4-hydroxyphenyl)acetyl]-N-(4-iodophenyl)piperidine-4-carboxamide; With sodium iodide; In N,N-dimethyl-formamide;

With potassium tert-butylate; In tetrahydrofuran; N,N-dimethyl-formamide; Cooling with ice;

chloro-methylsulfanyl-methane; In tetrahydrofuran; N,N-dimethyl-formamide; at 20 ℃; Cooling with ice;

Reference yield: 67.0%

: 1160707-36-7
1-[2-hydroxy-2-(4-(methylthiomethoxy)phenyl)acetyl]-N-(4-iodophenyl)piperidine-4-carboxamide

: 1160707-37-8
1-[2-hydroxy-2-(4-azidomethoxyphenyl)acetyl]-N-(4-iodophenyl)piperidine-4-carboxamide

Guidance literature:: 1-[2-hydroxy-2-(4-(methylthiomethoxy)phenyl)acetyl]-N-(4-iodophenyl)piperidine-4-carboxamide; With N-chloro-succinimide; chloro-trimethyl-silane; In dichloromethane; for 1.5h;

With sodium azide; In water; N,N-dimethyl-formamide; at 20 ℃; for 1.5h;
DOI:10.1039/c2cc37826d

Reference yield:

: 1160707-36-7
1-[2-hydroxy-2-(4-(methylthiomethoxy)phenyl)acetyl]-N-(4-iodophenyl)piperidine-4-carboxamide

: C₂₁H₂₂ClIN₂O₄

Guidance literature:: 1-[2-hydroxy-2-(4-(methylthiomethoxy)phenyl)acetyl]-N-(4-iodophenyl)piperidine-4-carboxamide; With N-chloro-succinimide; In dichloromethane;

With chloro-trimethyl-silane; In dichloromethane;