[Cu(N-2-hydroxy-naphthaldehyde-1-alkenyl-o-amino acid-2H)](n)

Base Information

Chemical Name:[Cu(N-2-hydroxy-naphthaldehyde-1-alkenyl-o-amino acid-2H)](n)
CAS No.:344792-35-4
Molecular Formula:C₁₈H₁₁NO₃*Cu
Molecular Weight:352.836
Hs Code.:

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Chemical Property of [Cu(N-2-hydroxy-naphthaldehyde-1-alkenyl-o-amino acid-2H)](n)

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Technology Process of [Cu(N-2-hydroxy-naphthaldehyde-1-alkenyl-o-amino acid-2H)](n)

There total 2 articles about [Cu(N-2-hydroxy-naphthaldehyde-1-alkenyl-o-amino acid-2H)](n) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 57.2%

: 796-47-4
2-[(2-hydroxynaphthalen-1-ylmethylene)amino]benzoic acid

: 6046-93-1
copper(II) acetate monohydrate

: 344792-35-4
[Cu(N-2-hydroxy-naphthaldehyde-1-alkenyl-o-amino acid-2H)](n)

Guidance literature:: In N,N-dimethyl-formamide; Cu-salt was added to a stirred soln. of DMF containing amino acid, the mixt. was refluxed under stirring for 4 h; ppt. was filtered, dissolved in min DMF and pyridine, diffusion of diethyl ether for two months; elem. anal.;
DOI:10.1016/j.molstruc.2011.04.025

Reference yield:

: copper(ll) sulfate pentahydrate

: 118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4
anthranilic acid

: 708-06-5
2-hydroxynaphthalene-1-carbaldehyde

: 344792-35-4
[Cu(N-2-hydroxy-naphthaldehyde-1-alkenyl-o-amino acid-2H)](n)

Guidance literature:: With LiOH; In methanol; High Pressure; HOC10H6CHO added to MeOH soln. contg. NH2C6H4COOH and LiOH; refluxed for2 h; CuSO4*5H2O in MeOH added; placed into stainless steel vessel; heat ed at 85°C for 6 d; cooled to room temp.; crystals collected; washed with MeOH; dried at ambient temp.; elem. anal.;
DOI:10.1016/j.molstruc.2007.02.009