ethyl N-(3-cyano-4-neopentyloxyphenyl)glycine

Base Information

Chemical Name:ethyl N-(3-cyano-4-neopentyloxyphenyl)glycine
CAS No.:288251-73-0
Molecular Formula:C₁₆H₂₂N₂O₃
Molecular Weight:290.362
Hs Code.:

Synonyms:

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Chemical Property of ethyl N-(3-cyano-4-neopentyloxyphenyl)glycine

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Technology Process of ethyl N-(3-cyano-4-neopentyloxyphenyl)glycine

There total 6 articles about ethyl N-(3-cyano-4-neopentyloxyphenyl)glycine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: ethyl N-tert-butoxycarbonyl-N-(3-cyano-4-neopentyloxyphenyl)glycine

: 288251-73-0
ethyl N-(3-cyano-4-neopentyloxyphenyl)glycine

Guidance literature:: With trifluoroacetic acid; at 20 ℃; for 1h;

Reference yield:

: 16588-15-1
2-chloro-5-nitro-benzamide

: 288251-73-0
ethyl N-(3-cyano-4-neopentyloxyphenyl)glycine

Guidance literature:: Multi-step reaction with 6 steps

1.1: benzenesulfonyl chloride / DMF (N,N-dimethyl-formamide); toluene / 3 h / 20 - 145 °C

2.1: sodium hydride / DMF (N,N-dimethyl-formamide) / 1 h / Ice cooling

3.1: iron; ammonium chloride / ethanol; water / 0.83 h / 65 °C / Heating / reflux

4.1: triethylamine / tetrahydrofuran / 4 h / 20 °C / Ice cooling

5.1: sodium hydride / DMF (N,N-dimethyl-formamide) / 1.5 h / 20 °C / Cooling with ice

5.2: 1 h / Cooling with ice

6.1: trifluoroacetic acid / 1 h / 20 °C

With iron; sodium hydride; ammonium chloride; triethylamine; benzenesulfonyl chloride; trifluoroacetic acid; In tetrahydrofuran; DMF (N,N-dimethyl-formamide); ethanol; water; toluene;

Reference yield:

: 206885-36-1
5-amino-2-neopentyloxybenzonitrile

: 288251-73-0
ethyl N-(3-cyano-4-neopentyloxyphenyl)glycine

Guidance literature:: Multi-step reaction with 3 steps

1.1: triethylamine / tetrahydrofuran / 4 h / 20 °C / Ice cooling

2.1: sodium hydride / DMF (N,N-dimethyl-formamide) / 1.5 h / 20 °C / Cooling with ice

2.2: 1 h / Cooling with ice

3.1: trifluoroacetic acid / 1 h / 20 °C

With sodium hydride; triethylamine; trifluoroacetic acid; In tetrahydrofuran; DMF (N,N-dimethyl-formamide);