zinc(II) complex with triphenyltetrabenzoporphine

Base Information

Chemical Name:zinc(II) complex with triphenyltetrabenzoporphine
CAS No.:120389-74-4
Molecular Formula:C₅₄H₃₂N₄Zn
Molecular Weight:802.265
Hs Code.:

Synonyms:

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Chemical Property of zinc(II) complex with triphenyltetrabenzoporphine

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Technology Process of zinc(II) complex with triphenyltetrabenzoporphine

There total 5 articles about zinc(II) complex with triphenyltetrabenzoporphine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 10.0%

: 103-82-2
phenylacetic acid

: 5970-45-6
zinc(II) acetate dihydrate

: 3,3-[1-(1-oxo-1H-isoindol-3-yl)methylene]-2,3-dihydro-1H-isoindol-1-one

: 120389-73-3
zinc(II) complex with monophenyltetrabenzoporphine

: 120389-74-4
zinc(II) complex with triphenyltetrabenzoporphine

: 80529-82-4
zinc(II) tetraphenyltetrabenzoporphinate

Guidance literature:: In neat (no solvent); byproducts: (meso-diphenyltetrabenzoporphinato)zinc(II); mixt. of starting materials heated to 350°C; kept for 25 min at this temp.; cooled; extracted (benzene); extract evapd. to dryness; dissolved (benzene); complexes sepd. by chromy. (Al2O3, as eluent benzene-hexane, benzene-hexane-acetone, benzene-hexane-ethyl acetate); elem. anal.;
DOI:10.1023/A:1020715202738

Reference yield: 5.0%

: 103-82-2
phenylacetic acid

: 136918-14-4,85-41-6
phthalimide

: 3,3-[1-(1-oxo-1H-isoindol-3-yl)methylene]-2,3-dihydro-1H-isoindol-1-one

: zinc(II) oxide

: 120389-74-4
meso-triphenyltetrabenzoporphine

Guidance literature:: In solid; a mixt. of ligands and ZnO was placed in a quartz test tube, heated to 360°C, and kept for 15 min; melt was cooled, crushed; product isolated by chromy. on Al2O3; identified by elem. anal. and UV spectrum;

Reference yield: 3.0%

: 1074-82-4
potassium phtalimide

: zinc(II) phenylacetate

: 132040-17-6
zinc(II) complex with trans-diphenyltetrabenzoporphine

: 132040-16-5
meso-diphenyltetrabenzoporphyrin zinc

: 120389-74-4
zinc(II) complex with triphenyltetrabenzoporphine

: 80529-82-4
zinc(II) tetraphenyltetrabenzoporphinate

Guidance literature:: In solid; well ground mixt. of potassium phthalimide salt and Zn(OCH2Ph)2 was heated at 360°C for 1 h under N2; extd. with hot dioxane and purified by column chromy. and PTLC on Al2O3 (benzene-hexane), septd. on Al2O3 (benzene-hexane-THF); isomers of meso-diphenyltetrabenzoporphinato zinc (2%) not septd.; contaminated with benzyl adducts (3D-HLPC and FD-MS data);
DOI:10.1016/S0020-1693(00)87937-2