(2,4-dimethoxyphenyl)(3-phenyloxiran-2-yl)methanone

Base Information

• Chemical Name: (2,4-dimethoxyphenyl)(3-phenyloxiran-2-yl)methanone
• CAS No.: 54305-70-3
• Molecular Formula: C₁₇H₁₆O₄
• Molecular Weight: 284.312

Synonyms:Methanone,(2,4-dimethoxyphenyl)(3-phenyloxiranyl)- (9CI); Propiophenone,2,3-epoxy-2',4'-dimethoxy-3-phenyl- (7CI); Propiophenone, a,b-epoxy-2,4-dimethoxy-b-phenyl- (2CI); 2',4'-Dimethoxychalcone epoxide

Chemical Property of (2,4-dimethoxyphenyl)(3-phenyloxiran-2-yl)methanone

Chemical Property:

• Vapor Pressure: 7.51E-09mmHg at 25°C
• Boiling Point: 465.7°C at 760 mmHg
• Flash Point: 208°C
• Density: 1.217g/cm³

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of (2,4-dimethoxyphenyl)(3-phenyloxiran-2-yl)methanone

There total 2 articles about (2,4-dimethoxyphenyl)(3-phenyloxiran-2-yl)methanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

→ 1-(2,4-dimethoxy-phenyl)-2,3-epoxy-3-phenyl-propan-1-one (54305-70-3)

Guidance literature:

With methanol; sodium hydroxide; dihydrogen peroxide;

DOI:10.1039/jr9320001798

Reference yield:

benzaldehyde (100-52-7) → 1-(2,4-dimethoxy-phenyl)-2,3-epoxy-3-phenyl-propan-1-one (54305-70-3)

Guidance literature:

With sodium ethanolate;

Reference yield: 90.0%

methanol (67-56-1) + 1-(2,4-dimethoxy-phenyl)-2,3-epoxy-3-phenyl-propan-1-one (54305-70-3) → (2R,3S)-1-(2,4-Dimethoxy-phenyl)-2-hydroxy-3-methoxy-3-phenyl-propan-1-one

Guidance literature:

With sulfuric acid; for 24h;

DOI:10.1016/j.tetlet.2006.06.107

upstream raw materials:

benzaldehyde

Downstream raw materials:

1-(2,4-dimethoxy-phenyl)-3-phenyl-propane-1,2-dione

3-chloro-1-(2,4-dimethoxy-phenyl)-2-hydroxy-3-phenyl-propan-1-one

1-(2,4-dimethoxy-phenyl)-2-hydroxy-3-methoxy-3-phenyl-propan-1-one

2-(2,4-dimethoxy-phenyl)-2-hydroxy-3-phenyl-propionic acid

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